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The relationship between the composition, coating microstructure and electromagnetic properties of electroforming Ni-Fe alloys was studied in this paper. And the optimal process parameters to obtain Ni-20%Fe deposition was as following: FeSO4•7H20 concentration was 6 g/L; PH value of the solution was 2.5; current density was 3.5 A/dm2; electrolyte temperature 55 °C. The results indicate that the Ni-Fe deposit is bright and compact, the crystal-planes of the plating were (111), (220) and (200). Electrodeposited Ni-20%Fe has a strong paramagnetism effect with the smallest remanence of 0.5 emu, The coercivity show a monotonic decrease with increasing Fe content in deposit, which proved that the electroformed Ni-20%Fe alloy has good electromagnetic property and could be used in MEMS actuator manufacturing.

This study demonstrates the thermal actions of tert-butyl peroxybenzoate (TBPB) which is widely used in the plastic and rubber industries. The thermodynamic and kinetic analysis were performed on the basis of dynamic and adiabatic calorimetric applications which had been accepted as good assistants for investigating materials’ thermal decomposition. In essence, TBPB is reactive and exothermically unstable. Differential scanning calorimetry (DSC) and accelerating rate calorimeter (ARC) were employed to supply basic data and safety index. Experiments were taken under different scanning rates as well as various sample mass. The temperature and pressure curves of TBPB during decomposition were recorded. Based on the significant parameters calculated, self-accelerating decomposition temperature (SADT) of TBPB worked out was 50°C.