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Amorphous steel slag was blended with different concentrations of waste glass (20, 40, 50, 60, 70 wt.%) and SiC to obtain a composite. According to Hot Stage Microscopy images, slag-glass composite contractions started at 1050 ºC. scanning electron microscope micrographs of slag-SiC (foaming agent) composite revealed tunnel-like porosities of 500 to 1000 microns. Gaseous products of carbide decomposition led to the formation of these tunnel-like porosities. By adding up to 50 wt. % of waste glass to this composite and sintering at 1200 ° C, the size of cavities decreased by 10 times and achieved 50 microns to form spherical cavities. By increasing glass content, the total porosity of slag-glass-SiC increased to 80 wt.% followed by a decrease in the strength to 3.2 MPa. Having an overall density of 0.8 g/cm3, the slag-glass composite could be classified as a porous foam material. Pseudo Waltonite phase was also detected in this composite after sintering. [ABSTRACT FROM AUTHOR]

The purpose of this study was to evaluate the effect of glycyrol (tri-dentate, GLY) and ethylenediamine (doubledentate clay, en) chelating agents on phase and morphology changes of spinel nanoparticles synthesized by sol-gel method. Characterization of samples was performed by X-ray diffraction (XRD) and field-emission scanning electron microscope (FESEM) equipped with energy dispersive X-ray spectrometer (EDX). The results showed that both samples synthesized with GLY and en contain cubic spinel phase. The sample synthesized with ethylenediamine has a pyramidal morphology with particle size in the range of 20-25 nm whereas the specimen prepared with glycerol is spherical with particle size in the range of 20-25 nm. Finally, suggested mechanism for morphological changes of spniel nanoparticles was discussed. [ABSTRACT FROM AUTHOR]