1. Comparison of electrolytic etching and immersion etching for 304L, 316L and 347 austenitic stainless-steel grades
- Author
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Nagar, R., Singh, R., Patil, N., and Yadav, I.
- Abstract
The aim of the work is to prepare and observe the metallographic specimen of 304L, 316L and 347 ASS samples with two different etching techniques. The samples were prepared by cutting, coarse grinding at 80 grit paper followed by fine grinding with 800, 1000, 1500, 2000 grit paper, polishing with diamond paste and kerosene on a velvet cloth. Later the samples were etched in aqua regia by immersion for 1 minute and in oxalic acid for electrolytic etching for 1 minute. The structure was observed at two different magnifications, 100× and 400×, using a light microscope. Electrolytic etching showed better results compared to the immersion technique. The structure was uniformly etched and had uniform light reflection. In addition to the clear structure, other particle phases were clearly visible. The 304L structure was fine grained as compared to 316L and 347 ASS. The structure observed was equiaxed austenite grains, annealed twins and particles.
- Published
- 2024
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