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The microstructures and mechanical properties of dissimilar weld joints between T92 and Super 304H steels were investigated. Dissimilar weld joints with four groove angles were constructed using gas tungsten arc welding. The results showed that post-weld heat treatment improved the mechanical properties of the dissimilar weld joints. The optimal groove angle for T92/Super 304H dissimilar weld joints was found to be 20°, considering mechanical properties. Furthermore, the transformation from equiaxed dendrites to columnar dendrites was observed in the weld metal. Epitaxial growth and delta ferrites were found around the fusion line between the Super 304H and the weld metal.