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LiNi 0.5 Mn 1.5 O 4 (LNMO), a next-generation high-voltage battery material, is promising for high-energy-density and power-density lithium-ion secondary batteries. However, rapid capacity degradation occurs due to problems such as the elution of transition metals and the generation of structural distortion during cycling. Herein, a new LNMO material was synthesized using the Taylor-Couette flow-based co-precipitation method. The synthesized LNMO material consisted of secondary particles composed of primary particles with an octahedral structure and a high specific surface area. In addition, the LNMO cathode material showed less structural distortion and cation mixing as well as a high cyclability and rate performance compared with commercially available materials., Competing Interests: The authors declare that the research was conducted in the absence of any commercial or financial relationships that could be construed as a potential conflict of interest., (Copyright © 2023 Lee, Song, Lee, Kim and Lim.)

Continuous slug flow in microreactors are featured by alternative presence of regulate segments of immiscible phases in microchannel or capillaries with lateral dimensions below 1 mm. Due to the high interfacial area and short diffusive distance therein, such microreactors have been widely applied in chemical engineering processes that are sensitive to mass transfer. Therefore, mass transfer rates in microreactors have long been broadly investigated via either typical offline or online methods. Compared to these conventional methods, the colorimetric technique based on the oxidation of resazurin with oxygen enables direct determination of physical mass transfer rates. However, this technique was currently applied only to the gas-liquid system in microreactors, and mostly in rectangular channels due to the simplicity in image processing. Based on this, the current paper showed a demo where the colorimetric technique using resazurin was adapted to a liquid-liquid system for the mass transfer study of flowing droplets within a slug flow capillary. Experimental tips and tricks were summarized, and a sliced color-concentration calibration strategy was proposed to balance analyzing efficiency and accuracy., Competing Interests: The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper. The authors declare the following financial interests/personal relationships which may be considered as potential competing interests., (© 2021 The Author(s).)

Nanoparticles as an application platform for active ingredients offer the advantage of efficient absorption and rapid dissolution in the organism, even in cases of poor water solubility. Active substances can either be presented directly as nanoparticles or can be integrated in a colloidal carrier system (e.g., lipid nanoparticles). For bottom-up nanoparticle production minimizing particle contamination, precipitation processes provide an adequate approach. Microfluidic systems ensure a precise control of mixing for the precipitation, which enables a tunable particle size definition. In this work, a gas/liquid Taylor flow micromixer made of chemically inert glass is presented, in which the organic phases are injected through a symmetric inlet structure. The 3D structuring of the glass was performed by femtosecond laser ablation. Rough microchannel walls are typically obtained by laser ablation but were smoothed by a subsequent annealing process resulting in lower hydrophilicity and even rounder channel cross-sections. Only with such smooth channel walls can a substantial reduction of fouling be obtained, allowing for stable operation over longer periods. The ultrafast mixing of the solutions could be adjusted by simply changing the gas volume flow rate. Narrow particle size distributions are obtained for smaller gas bubbles with a low backflow and when the rate of liquid volume flow has a small influence on particle precipitation. Therefore, nanoparticles with adjustable sizes of down to 70 nm could be reliably produced in continuous mode. Particle size distributions could be narrowed to a polydispersity value of 0.12.