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In fiber-reinforced polymer composites, the fiber-matrix interface controls stress transfer mechanisms, thereby affecting mechanical performance. Interfacial properties are often extracted via single-fiber composite tests. In these tests, the load is transferred from the polymer to the fiber through interfacial shear stresses, necessitating the evaluation of interfacial shear properties. To adopt these properties in the design of industrially relevant composites, one must assume that the damage mechanisms in single-fiber composites are representative of those in multi-fiber composites, consisting of highly aligned, unidirectional plies with high fiber volume fractions. That assumption, however, has never been validated. In this paper, the real-time damage development is monitored in single-fiber and multi-fiber composites using in situ X-ray holo-tomography at 150-nm pixel size. The technique enables the first-ever 3D detection of longitudinal interfacial debonding in carbon and glass single-fiber composites. This mechanism is not detected in multi-fiber composite specimens, suggesting that single-fiber composites are intrinsically unrepresentative of realistic composite behavior., (© 2024 Wiley‐VCH GmbH.)

Carbon fiber-reinforced polymer (CFRP) composite materials are widely used in engineering applications, but their production generates a significant amount of waste. This paper aims to explore the potential of incorporating mechanically recycled aerospace prepreg waste in thermoplastic composite materials to reduce the environmental impact of composite material production and promote the use of recycled materials. The composite material developed in this study incorporates a bio-based thermoplastic polymer, polyamide 11 (PA11), as the matrix material and recycled aerospace prepreg waste quasi-one-dimensionally arranged as reinforcement. Mechanical, thermal, and thermomechanical characterizations were performed through tensile, flexural, and impact tests, as well as differential scanning calorimetry (DSC) and dynamic mechanical analysis (DMA). Compared to previous studies that used a different recycled CFRP in the shape of rods, the results show that the recycled prepregs are a suitable reinforcement, enhancing the reinforcement-matrix adhesion and leading to higher mechanical properties. The tensile results were evaluated by SEM, and the impact tests were evaluated by CT scans. The results demonstrate the potential of incorporating recycled aerospace prepreg waste in thermoplastic composite materials to produce high-performance and sustainable components in the aerospace and automotive industries.

Fibre breaks govern the strength of unidirectional composite materials under tension. The progressive development of fibre breaks is studied using in situ X-ray computed tomography, especially with synchrotron radiation. However, even with synchrotron radiation, the resolution of the time-resolved in situ images is not sufficient for a fully automated analysis of continuous mechanical deformations. We therefore investigate the possibility of increasing the quality of low-resolution in situ scans by means of super-resolution (SR) using 3D deep learning techniques, thus facilitating the subsequent fibre break identification. We trained generative neural networks (GAN) on datasets of high-(0.3 μm) and low-resolution (1.6 μm) statically acquired images. These networks were then applied to a low-resolution (1.1 μm) noisy image of a continuously loaded specimen. The statistical parameters of the fibre breaks used for the comparison are the number of individual breaks and the number of 2-plets and 3-plets per specimen volume. The fully automated process achieves an average accuracy of 82% of manually identified fibre breaks, while the semi-automated one reaches 92%. The developed approach allows the use of faster, low-resolution in situ tomography without losing the quality of the identified physical parameters.

Understanding the fatigue behaviour of hybrid fibre-reinforced plastics is desirable for exploiting their features in safe, durable and reliable industrial components. The fatigue performance of hybrid composites has not been extensively investigated yet. The paper presents an overview of the available knowledge on the fatigue of hybrid fibre-reinforced plastics, and, more specifically, reports the fatigue behaviour of a quasi-isotropic pseudo-ductile all-carbon fibre interlayer hybrid composite by experimental measurements and observations, with emphasis on the damage development. The fatigue conditions are tension-tension stress- and strain-controlled cyclic loading. The results include fatigue life for different maximum stress and strain levels, stiffness evolution and damage observations by X-ray micro-computed tomography. The studied hybrid all-carbon fibre quasi-isotropic composite exhibits pseudo-ductility in quasi-static testing. For stress-controlled fatigue, the fatigue load over the limit of elastic response is not sustained. Contrary to that, the composite retains its load-carrying ability in the pseudo-ductile regime for a strain-controlled regime, albeit with lowered stiffness. This article is part of the theme issue 'Ageing and durability of composite materials'.

The increasing use of carbon fiber and epoxy resin composite materials yields an increase in the amount of waste. Therefore, we present a solution consisting of composites manufactured by hot pressing, employing polyamides (either PA11 or PA12) and a mechanically recycled carbon fiber-reinforced polymer (CFRP) as reinforcement. The main objectives are to study the manufacturing of those composites, to evaluate the fiber distribution, and to perform a mechanical, dynamical, and thermomechanical characterizations. The X-ray micro-computed tomography (μCT) shows that the fibers are well-distributed, maintaining a homogeneous fiber volume fraction across the material. The variability in the results is typical of discontinuous fiber composites in which the fibers, although oriented, are not as homogeneously distributed as in a continuous fiber composite. The mechanical and dynamic properties barely differ between the two sets of composites. A dynamic-mechanical analysis revealed that the glass transition temperature (T g ) increases slightly for both composites, compared to the polymers. These results illustrate the viability of the recycling and reuse route for preventing the deterioration of carbon fibers and promoting the subsequent reduction in the environmental impact by employing a thermoplastic matrix., Competing Interests: The authors declare no conflict of interest. The funders had no role in the design of the study; in the collection, analyses, or interpretation of data; in the writing of the manuscript; or in the decision to publish the results.

We performed in-situ tensile tests on two carbon fibre/epoxy composites with continuous scanning using synchrotron computed tomography (CT). Both composites were cross-ply laminates, and two specimens were tested for each composite. The voxel size was sufficiently small to recognize individual fibres and fibre breaks. For each test, 16-19 volumes were reconstructed, cropped down to the 0° plies and analysed to track fibre break and cluster development. This dataset provides the last CT volume before failure for each of the four specimens as well as the individual fibre break locations in all reconstructed volumes. These data are then plotted against predictions from six state-of-the-art strength models. The target is that these data become a benchmark for the development of new models, inspiring researchers to set up refined experiments and develop improved models., Competing Interests: The authors declare that they have no known competing financial interests or personal relationships which have, or could be perceived to have, influenced the work reported in this article., (© 2021 Published by Elsevier Inc.)

This data article presents fibre mechanical properties acquired using automated single fibre tensile testing equipment. The raw data consists of the fibre diameter, gauge length and load-displacement diagrams. A total of 690 fibres were tested across four carbon and one glass fibre type. The largest dataset, for the T700S carbon fibre, consists of 217 data points. After performing a compliance calibration, the load-displacement diagrams are converted into stress-strain diagrams from which the tensile modulus and strength are extracted. The data presented in this article can be used as input data for models or for data processing during determination of other properties experimentally. The interpretation of the data can be found in [1]. The data is hosted in the Mendeley Data repository at [2]., Competing Interests: The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper., (© 2021 The Author(s). Published by Elsevier Inc.)

We have performed synchrotron computed tomography on two different fiber-reinforced composites while they were being continuously in-situ loaded in 0° tension. One material is a glass/epoxy laminate and the other is a carbon/epoxy laminate. The voxel size is 1.1 µm, which allows clear recognition of the glass fibers, but not distinct individual carbon fibers. For each material, four loading steps are selected with approximately 0, 40, 73, and 95% of the failure load, and the 3D images of the four volumes from each material are overlaid. A volume of interest in the middle 0° ply is chosen and located in the 3D image of each loading step (Fig. 1). The cropped volumes of interest for each material are presented in this publication and are publicly available on Mendeley Data [1]. As examples of two frequently-used type of unidirectional fiber-reinforced composites, the presented data can be used for different microstructural analyses, including investigation of the 3D variability in fiber distribution and orientation, and their evolution during tensile loading. For example, we have performed fiber orientation analysis on this data, using our digital image correlation-based technique, in [2]. Moreover, real-time formation of fiber breaks with tensile loading can be investigated in the data., Competing Interests: The authors declare that they have no known competing financial interests or personal relationships which have, or could be perceived to have, influenced the work reported in this article., (© 2020 The Author(s).)

Increasing the efficiency of wind turbines will be vital for the wind energy sector to continue growing. The drive for increased efficiency is pushing turbine manufacturers to shift from glass fibre composite blades towards carbon/glass fibre-hybrid composite blades. This shift brings significant challenges in terms of optimising the design and understanding the failure of these new blade materials. This review therefore surveys the literature on fibre-hybrid composites, with an emphasis on aspects that are relevant for turbine blade materials. The literature on tensile, flexural, compressive, and fatigue performance is critically assessed and areas for future research are identified. Numerical simulations of fibre-hybrid composites have reached a reasonable maturity for tensile failure, but significant progress is required for flexural, compressive, and fatigue failure. Fatigue failure of fibre-hybrid composites in particular, requires more careful attention from both a modelling and experimental point of view., Competing Interests: The author declares no conflict of interest.