1. Effect of chemical surface treatment of titanium on its bond with dental ceramics.
- Author
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Parchańska-Kowalik M, Wołowiec-Korecka E, and Klimek L
- Subjects
- Air Abrasion, Dental, Aluminum Oxide, Dental Prosthesis, Humans, Surface Properties, Ceramics therapeutic use, Dental Bonding, Metal Ceramic Alloys therapeutic use, Titanium
- Abstract
Statement of Problem: Airborne-particle abrasion of titanium is a clinically accepted method of surface preparation. As a side effect of airborne-particle abrasion, particles of the abrasive material get embedded into the surface. How particle presence or removal from the titanium surface affects the strength of the titanium-ceramic bond is unclear., Purpose: The purpose of this in vitro study was to determine the effect of removing Al
2 O3 particles embedded into the surface by means of chemical surface treatment on the strength of the titanium-ceramic bond., Material and Methods: Titanium (TritanCpTi 1, Dentaurum, 99.5% Ti) disks were airborne-particle abraded with 110 μm Al2 O3 at a pressure of 0.4 MPa and an angle of approximately 45 degrees. The surface was etched chemically using 1 of 8 reagents, and the veneering ceramic applied and fired. The strength of the metal-ceramic bond was determined using the shear strength test. Further, the effect of thermal fatigue on the bond strength was evaluated. The results were analyzed with 2-way ANOVA and the Tukey honest significant difference (HSD) test (α=.05). Fractographic investigations and microscopic tests were also performed to determine the quality of the titanium-ceramic bond., Results: Effective etching of the titanium surface and removal of Al2 O3 particles included a 30% water solution of HNO3 + 3% HF, a mixture of HNO3 + HF + glycerin, a 4% solution of HF in H2 O2 , and a 4% solution of HF in H2 O. A statistically significant difference (of about 50%) in bond strength was found between the groups subjected to chemical etching and the control group (P<.05). Additionally, a statistically significant difference (about 25%) was found after thermocycling (P<.05)., Conclusions: Removing the Al2 O3 particles embedded into the titanium surface after airborne-particle abrasion lowers the strength of the titanium-ceramic bond (P<.05). Thermocycling also weakens the strength of the titanium-ceramic bond, regardless of the surface preparation (P<.05)., (Copyright © 2018 Editorial Council for the Journal of Prosthetic Dentistry. Published by Elsevier Inc. All rights reserved.)- Published
- 2018
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