1. Physical, mechanical properties and antimicrobial analysis of a novel CaO·Al 2 O 3 compound reinforced with Al or Ag particles.
- Author
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Gómez de Saravia SG, Rastelli SE, Ortega-Avilés M, González-Morán CO, Rocha-Rangel E, and Miranda-Hernández JG
- Subjects
- Biocompatible Materials chemistry, Ceramics chemistry, Elastic Modulus, Electrons, Hardness, Materials Testing, Microscopy, Microscopy, Electron, Scanning, Powders, Saliva microbiology, Scattering, Radiation, Staphylococcus drug effects, Stress, Mechanical, Tomography, X-Ray Computed, X-Ray Diffraction, Aluminum chemistry, Aluminum Compounds chemistry, Aluminum Oxide chemistry, Anti-Infective Agents pharmacology, Calcium Compounds chemistry, Oxides chemistry, Silver chemistry
- Abstract
Ceramic-metal (CaO·Al
2 O3 -Al and CaO·Al2 O3 -Ag) compounds were prepared by mechanical milling and consolidated through an in-situ sintering process. The aim of this work is to study the effects of the Al and Ag particles to ceramic-base compound, primarily in the microstructure, and its mechanical and antimicrobial properties. Chemical systems with a 1:1 M ratio between CaCO3 and Al2 O3 powder were formed, with the addition of 10 wt% Al or 10 wt% Ag, respectively. The compound material that consolidated were microstructurally characterized through X-ray diffraction, scanning electron microscopy, optic microscopy, and X-ray computed tomography. In addition, the hardness, the fracture toughness, the transversal elastic modulus, and the antimicrobial property were evaluated. The results of X-ray diffraction identified the formation of the calcium aluminate phases, such as CaO·6Al2 O3 (hibonite:CA6), CaO·2Al2 O3 (grossite:CA2), and CaO·Al2 O3 (krotite:CA); as well as Al and Ag were identified in its respective system. In addition, the mechanical properties show changes compared to the reference material that was synthesized under the same conditions and, finally, these materials also have an antimicrobial effect, against the Staphylococcus bacterium that is common in the oral cavity, when studied in synthetic saliva., (Copyright © 2019 Elsevier Ltd. All rights reserved.)- Published
- 2019
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