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1. 2D-NMR strategy dedicated to the analysis of weakly ordered, fully deuterated enantiomers in chiral liquid crystals

Author

Lesot, Philippe, Sarfati, Muriel, Merlet, Denis, Ancian, Bernard, and Emsley, James W.; Timimi, Bakir A.

Subjects
Carbon compounds -- Research, Carbon compounds -- Chemical properties, Liquid crystals -- Research, Liquid crystals -- Chemical properties, Nuclear magnetic resonance spectroscopy -- Usage, Chemistry
Abstract

The (super 2)H-(super 13)C heteronuclear 2D method gives a useful way to overcome the lack of (super 2)H chemical shift dispersion in titled Q-COSY 2D spectra. Also, a simple strategy is presented to attribute the quadrupolar doublets for two enantiomers and therefore obtain two sets of coherent data, one for each enantiomer, that can be used for further calculations.

Published
2003

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