39 results on '"rapid heating"'
Search Results
2. Facile Synthesis and Characterization of Low-Dimensional Layered Y2O3 Nanosheets by a Rapid Heating Route.
- Author
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Wang, Hongjun, Yang, Shuning, Zeng, Xiong, Chen, Mengyao, Guo, Zicong, Mi, Pengtao, Zhou, Jing, and Zhu, Yuanyuan
- Subjects
YTTRIUM oxides ,NANOSTRUCTURED materials ,X-ray diffraction ,CRYSTAL structure ,YTTRIUM - Abstract
Low-dimensional yttrium oxide (Y
2 O3 ) nanostructures have garnered significant research interest due to their intriguing properties arising from the dimensional effect and the modulation of the band structure. However, the simple preparation of Y2 O3 nanosheets is rarely investigated due to the inherent limitations posed by the counterpart bulk cubic or monoclinic crystal structure. Herein, the low-dimensional layered Y2 O3 nanosheets are prepared by a facile route of rapid heating followed by centrifugation, in which its corresponding hydrous-chloride compound is used as the sole reagent. The formation stages of layered Y2 O3 nanosheets and corresponding mechanisms are elucidated in detail. The x-ray diffraction results confirm that the intermediate product after rapid heating is yttrium oxychloride (YOCl), which converts to the single-phase Y2 O3 with a 2D layered phase after centrifugation. In addition, the obtained Y2 O3 nanosheets possess a direct optical bandgap of 5.49 eV, and thus may hold promise for use in electronic applications. This research provides a facile and low-cost method for the preparation of other low-dimensional nanosheets with similar structures. [ABSTRACT FROM AUTHOR]- Published
- 2024
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3. Intercalated Multilayer Graphene with Ultra Low Resistance for Next-Generation Interconnects.
- Author
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Huang, Jian-Zhi, Chang, En-Cheng, Tsao, Po-Chou, Ni, I-Chih, Li, Shu-Wei, Chan, Yu-Chen, Yang, Shin-Yi, Lee, Ming-Han, Shue, Shau-Lin, Chen, Mei-Hsin, and Wu, Chih-I
- Abstract
In recent years, many reports have demonstrated the high potential for multilayer graphene in semiconductor fabrication. As interconnects within semiconductors or electrodes for two-dimensional transistors, the preparation of large-area multilayer graphene is becoming increasingly important. Herein, we report a method for growing large-area multilayer graphene, which can achieve rapid heating and cooling. With the use of a high carbon concentration source, the preparation of multilayer graphene can be completed in a few seconds. This manufacturing method has the advantage of producing graphene with high quality, uniformity, and electrical conductivity. In commercial applications, this technology has great potential for the mass production and rapid fabrication of multilayer graphene. In addition, we found that the multilayer graphene produced by this method had cobalt atoms doped into the multilayer graphene during the process, resulting in its low resistivity. Combined with our intercalation technology, intercalated FeCl
3 in the graphene interlayer can reduce the resistivity of graphene to 3.55 μΩ cm, which is very close to the resistivity of copper bulk. This result makes multilayer graphene more promising for various applications. [ABSTRACT FROM AUTHOR]- Published
- 2023
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4. Realizing the Rapid Crystallization of YBa2Cu3O7-δ Films on LaMnO3 Buffer Layer by Induction Heating.
- Author
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Shen, Jia-Ji, Liu, Zhi-Yong, Chen, Jing, Zhou, Xing-Hang, Li, Yu-Gang, and Cai, Chuan-Bing
- Subjects
INDUCTION heating ,BUFFER layers ,SUPERCONDUCTING films ,CRYSTALLIZATION ,DISCONTINUOUS precipitation ,THIN films ,COPPER films - Abstract
YBa
2 Cu3 O7-δ (YBCO) thin films were fabricated rapidly on LaMnO3 /MgO/Y2 O3 /Al2 O3 /Hastelloy substrate by the self-built induction heating system. The growth rate can be more than 60 nm/s, which is much higher than the traditional Metal Organic Deposition (MOD) method. The effects of heating rate, oxygen partial pressure and growth temperature on the texture and morphology of YBCO films were studied, as well as the analysis of properties. The results of X-Ray Diffraction and Scanning Electron Microscopy demonstrated that rapid heating can effectively reduce the residual of BaCO3 particles. The faster heating rate results in a faster YBCO growth rate, easier c-axis oriented grains growth and denser morphology. Moreover, the growth temperature and atmosphere window of YBCO films were obtained in the rapid heating condition. Meanwhile, the YBCO nucleation and growth models were established. This work realized the rapid crystallization of YBCO films by induction heating system and improved understanding of the nucleation mechanism of YBCO on the flexible metal substrate with buffer layers, which is extremely attractive for the industrialization development of Fluorine Free-MOD superconducting films in the future. [ABSTRACT FROM AUTHOR]- Published
- 2022
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5. Experimental investigation on the effect of open fire on the tensile properties and damage evolution behavior of granite.
- Author
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Yin, Tubing, Yang, Zheng, Wu, You, Tan, Xiaosong, and Li, Mingjian
- Subjects
GRANITE ,FIRE exposure ,SCANNING electron microscopes ,ROCK properties ,TENSILE strength ,TUNNEL ventilation - Abstract
The stability of rock mass after fire is a concern of many engineering projects. In this paper, the effects of open fire and different cooling methods on granites were investigated. The static Brazilian test, dynamic Brazilian test, and P-wave velocity test were carried out to evaluate the mechanical properties and damage evolution behavior. A high-speed camera is employed to monitor the failure process of rock. The microstructures of the treated granites were observed by scanning electron microscope (SEM). The results showed that the fire duration and cooling treatment have a significant effect on the P-wave velocity, static nominal tensile strength, and dynamic nominal tensile strength of granite. These characteristics decrease rapidly during 0 to 10 min, and slowly decrease after 20 min. Compared to the air-cooling treatment, the water-cooling treatment has greater damage to the heated granite. To better understand the results, the rapid heating process of open fire heating was simulated using Abaqus software. The results reveal that there is a thinner compressive stress zone at the bottom of the specimen, and there is a large zone in the middle of the sample with higher tensile stress. The crack extension would be expanded due to high tensile stress, leading to the reduction of the tensile strength of the rock. This paper aims to better predict the degree of damage of rock materials after actual fire, as well as preliminarily explore the effect of the fire exposure duration and fire extinguishing method on the tensile properties of rock. [ABSTRACT FROM AUTHOR]
- Published
- 2022
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- View/download PDF
6. Applying rapid heating for controlling thermal displacement of CNC lathe.
- Author
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Van-The THAN, Chi-ChangWANG, Thi-Thao NGO, and Guan-Liang GUO
- Subjects
LATHE work ,MACHINE tools ,ELECTRIC heating systems ,TEMPERATURE control ,STEADY state conduction - Abstract
Thermal error always exists in a machine tool and accounts for a large part of the total error in the machine. Thermal displacement in X-axis on a CNC lathe controlled based on a rapid heating system is presented in this paper. Positive Temperature Coefficient (PTC) heating plates are installed on the X-axis of the machine. A control temperature system is constructed for rapid heating which further helps the thermal displacement to quickly reach stability. The system then continuously maintains stable compensation of the thermal error. The presented rapid heating technique is simpler than the compensation of machine thermal errors by interference in the numerical control system. Results show that the steady state of the thermal displacement in the X-axis can be acquired in a shorter time. In addition, thermal errors in constant and varying working conditions could be significantly reduced above 80% and 60%, respectively, compared to those without using the rapid heating. Therefore, the proposed method has a high potential for application on the CNC lathe machine for improving its precision. [ABSTRACT FROM AUTHOR]
- Published
- 2022
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7. Study on Filling Capacity of Optical Glass in a Novel Rapid Hot Embossing Process.
- Author
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Li, Jianzhi, Gong, Feng, Wang, Xin, and Yang, Gao
- Subjects
OPTICAL glass ,TEMPERATURE control ,TEMPERATURE distribution ,SILICON carbide ,GLASS - Abstract
This paper aims to present a novel rapid hot embossing approach and to study filling capacity of optical glass in the hot embossing process. Firstly, a novel rapid hot embossing device is developed, which consists of a rapid heating module and a precision loading module. Particularly, the rapid heating module allows a maximum temperature of 800 °C and a heating rate of 300 °C/min, with decent temperature control accuracy and uniform temperature distribution. In hot embossing process, by incompletely filling the microhole of silicon carbide mold, a microlens would be formed on the surface of glass disc, and the filling capacity of glass is quantified by the maximum height of the microlens. The tailor-made hot embossing device was exploited to conduct a series of experiments for evaluating effects of process parameters on the filling capacity of N-BK7 glass. Experimental results indicate that the filling capacity of glass could be enhanced by increasing the embossing force, the embossing temperature, the soaking time but decreasing the annealing rate. Furthermore, compared to soaking time and annealing rate, embossing force and embossing temperature have more significant influence on the filling capacity of N-BK7 glass. Therefore, the novel rapid hot embossing is a practical and promising technology for fabricating microstructures on glass materials with high softening points. [ABSTRACT FROM AUTHOR]
- Published
- 2022
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8. DC electric field‐assisted hot pressing of zirconia: Methodology, phenomenology, and sintering mechanism.
- Author
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Xu, Jingkun, Liu, Zetan, Xie, Zhipeng, He, Shan, and Xi, Xiaoqing
- Subjects
HOT pressing ,YTTRIA stabilized zirconium oxide ,SINTERING ,ATOMIC force microscopy ,ZIRCONIUM oxide ,CARRIER density - Abstract
Flash sintering (FS) is an important technique in the field of ceramic sintering. Nevertheless, conventional FS is less attractive for practical applications because of the complex shapes and small sizes of the specimens. In this study, using the novel electric field‐assisted hot pressing (FAHP) technique, we successfully achieved FS during the net‐shape hot pressing (HP) process for the first time. It was found that the 3 mol% yttria‐stabilized zirconia (3YSZ) can be flash sintered at 909°C using a fairly low DC field of 33 V/cm under 30 MPa pressure. The grain sizes of the FAHP‐sintered samples were 20% smaller than that of the HP‐sintered sample. When the current density limit is ≥240 mA/mm2, 3YSZ can be fully densified during the flash events. Careful analysis of the sintering curves suggests that although the carrier type or concentration is changed during flash events, it cannot explain the ultrafast densification. Additionally, we devised a qualitative method to analyze the densification mechanism. The results indicated that the ultrafast densification observed during flash events resulted from the synergistic effects of the rapid heating rate and peak sample temperature. Finally, the atomic force microscopy confirmed the lower grain boundary energy for the FAHP‐sintered samples, which accounts for the smaller grain sizes than the HP‐sintered sample. We believe that the FAHP technique could create new possibilities for theoretical and applied research on field‐assisted sintering techniques. [ABSTRACT FROM AUTHOR]
- Published
- 2021
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9. Effects of Rapid Infrared Heating and Cryogenic Cooling on the Tensile Properties and Fracture Behavior of Al-Cu-Mg.
- Author
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Ghannadi, Mitra, Hosseini, Hedieh, Sadeghi, Bagher Mohammad, Mirzakhani, Bahman, and Honaramooz, Mohammad Taha
- Subjects
INFRARED heating ,THERMODYNAMIC cycles ,NITROGEN in water ,COOLING ,HEAT treatment ,PRECIPITATION hardening ,TENSILE tests - Abstract
The objective of this work was to investigate the effect of rapid heating and cryogenic cooling on the fracture and tensile properties of Al-Cu-Mg samples. The specimens were subjected to three different heat treatment cycles in which the Infrared heating (IR) were used as the heating medium at the ageing stage, and the liquid nitrogen and water were used as the quenching mediums. The ageing temperature and time were 190⁰C and from 2 - to 10h respectively. The results indicated that by using IR at the ageing stage, the hardening rate enhanced because the rapid heating via this method led to faster diffusion of the alloying elements. Moreover, the high density of nanosized precipitates formed during ageing was another reason for higher strength and ductility. Cryogenic treatment had a negligible effect on both the microstructure and tensile properties. However there was an improvemnet in the ductility to some extent. Overall, the combination of a high heating rate and cryogenic treatment led to the highest mechanical properties. SEM micrographs of the fracture surface demonstrated that in Cryogenic treatment plus Artificial Ageing (CAA) condition, the surface was fully covered by deep dimples in contrast to the Cryogenic treatment plus Infrared Heating (CIR) and Water-Quench plus Infrared Heating (QIR) conditions which contained shallwer dimples. Some facets were also observed in the latter samples. [ABSTRACT FROM AUTHOR]
- Published
- 2021
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10. High-efficiency flow-through induction heating.
- Author
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Kilic, Veli Tayfun, Unal, Emre, and Volkan Demir, Hilmi
- Subjects
HEATING ,INDUCTION heating ,PLASTIC pipe ,HEAT transfer ,ENERGY transfer ,CALORIMETRY - Abstract
This study reports a newly designed induction heating system for efficient, fast, and safe flow-through heating. The system has a very simple architecture, which is composed of a transmitting coil, an isolating plastic pipe, and an embedded metal shell. Wireless energy transfer from the external coil to the internal metal shell through the pipe is essential for decreasing losses. Also, a large contact surface between a fluid and the immersed shell enables rapid heat transfer. The proposed heating system was systematically investigated for different shell geometries and the results were compared with a commercially available conductive flow-through heating device. As a proof-of-concept demonstration, a prototype of the designed induction heating system was manufactured and the heating measurements were conducted with water. Power transfer efficiency of the prototyped induction heating system was measured to be 97%. The comparative study indicates that such high-efficiency induction flow-through heating system offers a great potential for replacing the conventional conductive heating device used in household applications in which the rapid and compact heating is desired. [ABSTRACT FROM AUTHOR]
- Published
- 2020
- Full Text
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11. Interferometric Study of the Heat Transfer Phenomena Induced by Rapid Heating of Nickel Sheet.
- Author
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Seo, Hyeon-Seok, Hwang, In-Ju, and Kim, Youn-Jea
- Subjects
HEAT transfer ,COMPRESSIVE force ,HEAT ,NUSSELT number ,FORCED convection - Abstract
Visualization of the heat transfer phenomena induced by the rapid heating of nickel sheets was carried out using a Mach–Zehnder interferometer (MZI) and a high-speed camera. This phenomenon may be an important factor in heat transfer phenomena when the working fluids reach the thermodynamic critical point. The effect of heat transfer on the heating conditions of a nickel sheet was quantified by finite fringe analysis. The results show that isotherms near the heating surface with rapid heating are generated, and the induced isotherms are moved upward with similar patterns for different heating conditions. In addition, it is confirmed that the local Nusselt number decreases to the relationship of a secondary function if the thickness of the metal specimen is very thin and the time to reach the highest temperature is very short. Moreover, it decreased according to the increase of heating energy because the heat transfer mainly occurred by conduction and radiation rather than by convection, because the expansive force and compressive force between the fluid layers on the wall increased due to an increase in the heating energy in the beginning. [ABSTRACT FROM AUTHOR]
- Published
- 2020
- Full Text
- View/download PDF
12. Warm stamping of ultra-high strength steel sheets at comparatively low temperatures using rapid resistance heating.
- Author
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Mori, Ken-ichiro, Abe, Yohei, and Miyazawa, Sadao
- Subjects
LOW temperatures ,SHEET steel ,HEATING ,RESISTANCE heating ,FURNACES ,CORROSION resistance - Abstract
A warm stamping process of 1 and 1.2 GPa ultra-high strength steel sheets at comparatively low temperatures using rapid resistance heating was investigated to produce high strength parts. The effects of the heating temperature and rate on mechanical and surface properties of warm-stamped parts were examined. For a rapid heat rate of 100 °C/s around a heating temperature of 300 °C, the hardness of the formed parts increased from that of the as-received sheets, and the hardness for the 1.2 GPa sheet approached that of conventional hot-stamped parts from 22MnB5 steel sheets. The increase in hardness appeared only for rapid heating, and not for slow heating using a furnace. The increase in hardness is due to the transformation of retained austenite into martensite at comparatively low temperatures using rapid resistance heating and cooling. For the comparative low heating temperature, the non-coated sheet hardly oxidised, and the galvannealed sheet having high corrosion resistance did not exhibit the exfoliation of the coating layer, whereas the springback did not improve. [ABSTRACT FROM AUTHOR]
- Published
- 2020
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13. MICROSTRUCTURAL IMAGE ANALYSES OF MILD CARBON STEEL SUBJECTED TO A RAPID CYCLIC HEAT TREATMENT.
- Author
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Aghogho, Orhadahwe Thomas, Akanni, Adeleke Adekunle, Olayiwola, Aweda Jacob, Pelumi, Ikubanni Peter, and Odusote, Jamiu Kolawole
- Subjects
MILD steel ,CARBON steel ,HEAT treatment ,IMAGE analysis ,CARBON analysis - Abstract
The study is focused on using an image analysis to explain the effects of several cycles of rapid heat treatment on the microstructure of 0.213 wt. % carbon steel. The samples examined are subjected to a diffusional heat treatment followed by several cycles of a rapid heat treatment. The process of the diffusional heat treatment involves heating the samples from an ambient temperature to 850oC in an electric muffle furnace for 56 min and then quenching in running water. In order to improve further the mechanical properties of the heat treated samples, they are subjected to several cycles of rapid heating. Each cycle comprises preheating the furnace to 900oC prior to the samples charging. The treated samples are subjected to a microstructural examination using optical microscopy followed by an image analysis using Image J software. The mechanical properties of the heat treated samples are characterized through ultimate tensile, hardness and impact tests. The results reveal that the grain size decreases from 1.07 µm in the control sample to 0.79 µm in the three-cycle sample and increases to 0.86 µm in the four-cycle one. It is also observed that the two-cycle sample shows the highest ductility (15356.3 N/mm2) and the lowest ultimate strength (833.375 N/mm2). This implies that the two-cycle rapid heat treatment is required for grain refinement in mild carbon steel. [ABSTRACT FROM AUTHOR]
- Published
- 2020
14. Suppression of crystallization in ZBLAN glass by rapid heating and cooling processing.
- Author
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Ong, Teng‐Cheong, Fogarty, Ben, Steinberg, Ted, Jaatinen, Esa, and Bell, John
- Subjects
FLUORIDE glasses ,FOOD pasteurization ,HEAT conduction ,TRANSMISSION electron microscopy ,GLASS ,CRYSTALLIZATION - Abstract
ZBLAN glass is a heavy metal fluoride glass that tends to undergo heavy devitrification, resulting in a crystalline material. It has many applications, including its use as an optical waveguide for fiber‐optic technology. However, when the glass is processed with traditional casting techniques, crystallites form readily that act as scattering centers, which results in large attenuation losses. In this study, it has been experimentally demonstrated that processing ZBLAN rapidly with a heating rate of 25 000 K/min and cooling rate of 4000 K/min yields test samples that are fully amorphous and retain a disordered molecular arrangement characteristic of its molten state. This novel method was developed using a specifically designed equipment named a Rapid Electro‐thermal Processing Device, or "REPD." The REPD applies ohmic heating and thermal conduction to a heat sink to rapidly process the ZBLAN material. The absence of crystallites in the rapidly processed ZBLAN test samples were verified using transmission electron microscopy (TEM) analysis. Applying a theoretical algorithm, the critical cooling rate for yielding fully amorphous ZBLAN glass was determined to be 1081 K/min for a sample volume of 9.4 × 10−8 m3. [ABSTRACT FROM AUTHOR]
- Published
- 2019
- Full Text
- View/download PDF
15. Effects of Heating and Quenching Processing Parameters on Phase Transformation of 55CrMo Steel.
- Author
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Liu, Haijuan, Li, Huiping, Li, Zhichao, and He, Lianfang
- Subjects
HEATING ,QUENCHING (Chemistry) ,PHASE transitions ,CHROMIUM molybdenum steel ,MICROSTRUCTURE ,MICROHARDNESS ,AUSTENITE - Abstract
Microstructure and mechanical properties after induction hardening have a significant effect on the wear resistance performance and lifetime of 55CrMo steel ball screw. In the paper, the dilatometric curves were recorded at the different heating rate by a Gleeble-1500D thermo-mechanical simulator to determine the effect of heating rate on the austenitizing temperature of 55CrMo steel. Heat treatment of some specimens was performed by the Gleeble-1500D thermal simulator at the different heating temperature, holding time and cooling rate to investigate the effect of induction hardening parameters on the phase transformation, microstructure and microhardness of 55CrMo steel. Microstructure of specimen was analyzed using an optical microscope and a scanning electron microscope. Volume fraction of retained austenite was measured using an x-ray diffractometer. The mechanical properties were evaluated by a microhardness tester. The results show that the austenitizing temperature of 55CrMo steel increases with the increasing heating rate. Increasing the heating temperature, holding time and cooling rate of specimen is helpful in obtaining a uniform cryptocrystalline martensite. Volume fraction of retained austenite is less as the heating temperature is in the range of 900-950 °C. In the induction hardening of 55CrMo steel, the heating temperature should be in the range of 900-1000 °C. [ABSTRACT FROM AUTHOR]
- Published
- 2018
- Full Text
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16. Fast charging of lithium-ion batteries at all temperatures.
- Author
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Xiao-Guang Yang, Guangsheng Zhang, Shanhai Ge, and Chao-Yang Wang
- Subjects
LITHIUM-ion batteries ,TEMPERATURE ,ELECTRIC vehicles ,AUTOMOBILES ,ELECTROLYTES - Abstract
Fast charging is a key enabler of mainstream adoption of electric vehicles (EVs). None of today's EVs can withstand fast charging in cold or even cool temperatures due to the risk of lithium plating. Efforts to enable fast charging are hampered by the trade-off nature of a lithium-ion battery: Improving low-temperature fast charging capability usually comes with sacrificing cell durability. Here, we present a controllable cell structure to break this tradeoff and enable lithium plating-free (LPF) fast charging. Further, the LPF cell gives rise to a unified charging practice independent of ambient temperature, offering a platform for the development of battery materials without temperature restrictions. We demonstrate a 9.5 Ah 170 Wh/kg LPF cell that can be charged to 80% state of charge in 15 min even at -50 °C (beyond cell operation limit). Further, the LPF cell sustains 4,500 cycles of 3.5-C charging in 0 °C with <20% capacity loss, which is a 90x boost of life compared with a baseline conventional cell, and equivalent to >12 y and >280,000 miles of EV lifetime under this extreme usage condition, i.e., 3.5-C or 15-min fast charging at freezing temperatures. [ABSTRACT FROM AUTHOR]
- Published
- 2018
- Full Text
- View/download PDF
17. Investigation on Influence of Rapid Heating on Austenitization of Ultra-High Strength Steel.
- Author
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Tao, W. J., Liang, W. K., and Zhang, Y. S.
- Subjects
HIGH strength steel ,AUSTENITIC steel ,HEATING ,HEAT treatment of steel ,GRAIN size - Published
- 2016
18. The Evolution of Oxidation Scales on 22MnB5 Hot Press Forming Steel during Rapid Heating.
- Author
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Yao, S. J., Liu, W. J., Gao, W. B., Zhang, Z. W., and Ding, Y. L.
- Subjects
HOT pressing ,MANGANESE steel ,FOIL stamping ,HIGH strength steel ,AUTOMOBILE steel ,OXIDATION kinetics - Published
- 2016
19. Local out-of-plane deformation of CFRP ablator subjected to rapid heating.
- Author
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Koyanagi, Jun, Fukuda, Yasuhiro, Yoneyama, Satoru, Hirai, Ken-ichi, Yoshimura, Akinori, Aoki, Takuya, and Ogasawara, Toshio
- Subjects
CARBON fiber-reinforced plastics ,DEFORMATIONS (Mechanics) ,ABLATIVE materials ,THREE-dimensional imaging ,PYROLYSIS - Abstract
This study investigates local out-of-plane deformation of a carbon fiber reinforced phenolic polymer ablator subjected to very rapid heating. Local out-of-plane deformation was measured using a three-dimensional digital image correlation technique at high temperatures. This was achieved by attaching high temperature resistant random patterns on the specimen surface using a ceramic bond. Additionally, blue filters intended for cutting strong infrared radiation from the specimen were also used. This study then discusses the mechanisms of the local out-of-plane deformation under rapid heating conditions in terms of carbonization, pyrolysis gas occurrence, gas pressure storage, and interlaminar debonding due to gas pressure. [ABSTRACT FROM PUBLISHER]
- Published
- 2017
- Full Text
- View/download PDF
20. Improving the formability of linear flow split profiles by laser annealing.
- Author
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Niehuesbernd, J., Monnerjahn, V., Bruder, E., Groche, P., and Müller, C.
- Subjects
LASER annealing ,STEEL alloys ,MECHANICAL properties of metals ,TENSILE strength ,HARDENABILITY of metals ,RECRYSTALLIZATION (Metallurgy) - Abstract
Copyright of Materialwissenschaft und Werkstoffechnik is the property of Wiley-Blackwell and its content may not be copied or emailed to multiple sites or posted to a listserv without the copyright holder's express written permission. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)
- Published
- 2016
- Full Text
- View/download PDF
21. Origin of abnormal formation of pearlite in medium-carbon steel under nonequilibrium conditions of heating.
- Author
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Mirzaev, D., Yakovleva, I., Tereshchenko, N., Urtsev, V., Degtyarev, V., and Shmakov, A.
- Abstract
The structure and kinetics of the formation of austenite in medium-carbon steel during shortterm heating above the temperature Ac followed by accelerated cooling are analyzed. It has been shown that the abnormal formation of pearlite in steel results from the concentrational and structural inhomogeneity of austenite, as well as the presence of carbide particles in ferrite areas. [ABSTRACT FROM AUTHOR]
- Published
- 2016
- Full Text
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22. Rapid curing vacuum-assisted resin infusion molding using silicone rubber sheet heater and the effect of cooling process on the properties of carbon fiber/epoxy composites.
- Author
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Zhang, Kaomin, Gu, Yizhuo, Zhang, Jinglun, Li, Min, Wang, Shaokai, and Zhang, Zuoguang
- Subjects
CARBON fibers ,CURING ,SILICONE rubber ,EPOXY compounds ,COMPOSITE materials - Abstract
Silicone rubber sheet heater-aided vacuum-assisted resin infusion molding was developed in order to shorten curing cycle time. Three kinds of cooling methods, including air cooling, air water cooling, and water cooling, were employed; the effects of cooling process on processing time, residual strains, and mechanical properties were experimentally studied. The residual strains generated in cooling stage were monitored by embedded strain gauges. The results showed that in order to avoid serious residual strains and lower mechanical properties, the cooling rate of the silicone rubber sheet heater-aided vacuum-assisted resin infusion molding process should be designed carefully. Slow cooling rate before glass transition temperature of the composites and rapid cooling rate after it might be a practical method to maintain both high processing efficiency and acceptable mechanical properties. [ABSTRACT FROM AUTHOR]
- Published
- 2016
- Full Text
- View/download PDF
23. A novel ultrashort capillary gas chromatography method using on-column injection and detection.
- Author
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Alkhateeb, Fadi L., Hayward, Taylor C., and Thurbide, Kevin B.
- Subjects
GAS chromatography ,FLAME ionization detectors ,POLYPEPTIDES ,CHEMICAL decomposition ,HIGH performance liquid chromatography - Abstract
Copyright of Canadian Journal of Chemistry is the property of Canadian Science Publishing and its content may not be copied or emailed to multiple sites or posted to a listserv without the copyright holder's express written permission. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)
- Published
- 2016
- Full Text
- View/download PDF
24. Design of an induction heating coil coupled with magnetic flux concentrators for barrel heating of an injection molding machine.
- Author
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Hwang, Sheng-Jye and Bui, Huy-Tien
- Subjects
MACHINE molding (Founding) ,INDUCTION heating ,MAGNETIC flux ,INDUCTION coils ,RESISTANCE heating - Abstract
In an injection molding machine, the conventional barrel heating system which uses resistance heating method (RH) has some drawbacks such as low heating rate, long heating time, and energy loss. With induction heating (IH) technique, the barrel can better handle almost all of these disadvantages. However, non-uniform temperature distribution on inside surface of a barrel is the main drawback of induction heaters. A working coil coupled with magnetic flux concentrators via adjustment of magnetic flux concentrator spacing to achieve uniformity of magnetic flux and temperature distribution on the inside surface of a barrel was proposed and experimented. Results showed that, when barrel was heated by induction heating method with the proposed induction heating coil, heating time to reach a specific temperature could be reduced, and heating rate increased compared to resistance heating method. With 8 mm pitch of magnetic flux concentrators on a coil, the temperature distribution was the most uniform. [ABSTRACT FROM PUBLISHER]
- Published
- 2015
- Full Text
- View/download PDF
25. Initiation and Reaction in Al/Bi 2 O 3 Nanothermites: Evidence for the Predominance of Condensed Phase Chemistry.
- Author
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Piekiel, Nicholas W., Zhou, Lei, Sullivan, Kyle T., Chowdhury, Snehaunshu, Egan, Garth C., and Zachariah, Michael R.
- Subjects
CONDENSED matter ,ALUMINUM oxide ,BISMUTH oxides ,NANOPARTICLES ,HEATING ,TIME-of-flight mass spectrometry ,OXIDIZING agents - Abstract
This study explores the reaction between Al and Bi2O3nanoparticles under high heating rate conditions with temperature-jump/time of flight mass spectrometry (T-Jump/TOFMS), high speed imaging, and rapid sample heating within a scanning electron microscope (SEM). Comparison of rapid heating of Al/Bi2O3thermite and neat Bi2O3shows that initiation of the Al/Bi2O3reaction occurs at a much lower temperature than the point where oxygen is released from the neat Bi2O3powder. Thus, without the presence of a gas phase oxidizer, it can be concluded that a condensed phase initiation mechanism must be at play in the Al/Bi2O3nanothermite. C/Bi2O3heating experiments were used for a mechanistic comparison between two different fuel types since the carbon represents a nonvolatile fuel in contrast to the aluminum. This formulation showed a similar condensed phase initiation as was seen with the aluminum nanothermite. Qualitative comparison of high speed imaging for Al/Bi2O3and Al/CuO indicates that the initiation reaction in Al/Bi2O3is about twice as fast as a comparable copper oxide system, which has not been apparent from bulk thermite combustion studies. Bi2O3is known to possess unique ion transport properties, which combined with the presence of oxygen and aluminum ions within the nanothermite system may play a significant role in the speed of the nanothermite reaction. [ABSTRACT FROM AUTHOR]
- Published
- 2014
- Full Text
- View/download PDF
26. Rapid heating induced vibration of circular cylindrical shells with magnetostrictive functionally graded material.
- Author
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Hong, C. C.
- Subjects
ENGINEERED cylindrical shell vibration ,HEATING ,MAGNETOSTRICTION ,FUNCTIONALLY gradient materials ,HEAT flux - Abstract
The vibration and transient response of rapid heating on inner surface of the functionally graded material (FGM) circular cylindrical shells with outer magnetostrictive layer is investigated and computed by using the generalized differential quadrature (GDQ) method. The effects of heat flux value, power law index value, environmental temperature value and control gain value on Terfenol-D FGM circular cylindrical shell subjected to two edges clamped condition due to the not very high temperature fluid rapidly flow into the circular cylindrical shells from one side to the end of axial length direction are analyzed. The higher amplitudes of displacement and thermal stress can be obtained under the higher rapid heat flux value. With suitable product of coil constant and control gain value can reduce the amplitudes of displacement and thermal stress into a smaller value. The displacement of Terfenol-D FGM circular cylindrical shell versus the Terfenol-D thickness is stable for all power law index values. The Terfenol-D FGM circular cylindrical shell can stand against the higher temperature of environment with some values of power law index under rapid heating. [ABSTRACT FROM AUTHOR]
- Published
- 2014
- Full Text
- View/download PDF
27. Effect of quenching temperature on structure and properties of titanium alloy: Physicomechanical properties.
- Author
-
Popov, A., Illarionov, A., Stepanov, S., and Ivasishin, O.
- Abstract
Regularities of the formation of physicomechanical properties of the VT16 alloy (Ti-3.33Al-5.18Mo-4.57V, wt %) quenched after furnace and rapid heating have been established using optical microscopy, X-ray diffraction (XRD), and dynamic mechanical analysis. It has been shown that changes in the modulus of elasticity of the VT16 alloy correlate with a decrease in the volume fraction of the α phase in the structure, except for a slight increase in the modulus of elasticity (related to the presence of the ω phase) in the case when quenching temperatures of 800-825°C were used. It has been found that the use of rapid heating to the quenching temperature leads to an increase in the temperature of the alloy transition into the single-phase β state, hampers grain growth during heating for quenching at temperatures close to the polymorphic-transition temperature, and creates conditions for more efficient strengthening in the course of subsequent aging. [ABSTRACT FROM AUTHOR]
- Published
- 2014
- Full Text
- View/download PDF
28. Rapid heating effects on grain-size, texture and magnetic properties of 3% Si non-oriented electrical steel.
- Author
-
Wang, Jian, Li, Jun, Wang, Xinfeng, Mi, Xiaochuan, and Zhang, Shengen
- Subjects
HEATING ,MAGNETIC properties of metals ,SILICON compounds ,METAL microstructure ,ELECTRICAL steel ,X-ray diffraction ,ELECTROMAGNETIC induction - Abstract
The rapid heating effects on the microstructure, texture and magnetic properties of 3% Si non-oriented electrical steel has been investigated through optical microscopy, X-ray diffraction and Epstein frame. The results show that recrystallized grains were refined with increased heating rate, caused by the nucleation rate increase, which is faster than the growth rate due to rapid hearting. With the heating rate increase, the characteristic {111} recrystallization fibre of cold-rolled steel was depressed, but the beneficial 〈001〉//RD and 〈001〉//ND fibres were significantly strengthened. Although the grain-size decreases with heating rate increasing, the optimal magnetic properties can also be obtained through the recrystallized grain-size and texture optimization by rapid heating. In this research, we find the magnetic properties optimization can be obtained when annealed with 100°C/s heating rate: the core loss ( P) decrease 13% and the magnetic induction ( B) increase 3%. [ABSTRACT FROM AUTHOR]
- Published
- 2011
- Full Text
- View/download PDF
29. The Mechanical Response of Shape Memory Alloys Under a Rapid Heating Pulse.
- Author
-
Vollach, S. and Shilo, D.
- Subjects
SHAPE memory alloys ,ACTUATORS ,NUCLEATION ,ALLOYS ,MECHANICS (Physics) - Abstract
Shape memory alloy (SMA) actuators are very promising due to their large strain and work-output, but are considered to be very slow due to their cooling rate. In this article, we explore the capabilities of a fast one-directional actuation mode based on one-occasional rapid Joule heating of SMA elements. For this purpose, a unique experimental system has been developed that applies a high-voltage electric pulse to a detwined NiTi wire and measures the resulting displacement due to the martensite to austenite phase transformation. The electric pulse is tuned to produce variable temperature jump of up to 160°C within a risetime of few microseconds. One end of the wire is clamped while the displacement of the other end is monitored both by a laser doppler vibrometer and by an optical encoder that measures the displacement of a grating device. Analysis of experimental results reveals a dead time delay between the electric pulse and the wire’s response, which is attributed to the austenite nucleation time and which determines the limit on the fastest possible shape memory actuation. Further analysis reveals relations between the dead weight used and the average acceleration and maximal velocity obtained. In particular, the maximal velocity correlates to a constant kinetic energy delivered by the wire, which suggests a constant integrand over the stress-strain curve regardless of the dead-weight used. A comparison of actuation performances demonstrates that our actuation experiments are significantly advantageous over other fast actuation methods in almost every actuation aspect reviewed. This demonstrates the great potential of SMA for applications that require high speeds and large displacements one-occasional actuation. [ABSTRACT FROM AUTHOR]
- Published
- 2010
- Full Text
- View/download PDF
30. A zone-control induction heating (ZCIH) system for semiconductor processing.
- Author
-
Fujita, Hideaki, Ozaki, Kazuhiro, and Uchida, Naoki
- Subjects
INDUCTION heating ,ELECTRIC inverters ,ELECTRIC inductance ,ELECTRIC coils ,ELECTRIC heating - Abstract
This paper proposes a new induction heating technology capable of controlling a precise exothermic distribution, which is termed zone-control induction heating (ZCIH). The ZCIH system consists of two or more sets of a high-frequency inverter unit and a work coil. The inverter units control the phase angle of the coil current to be in phase with each other. The ZCIH has the capability of operation with the mutual inductance, and enables locating the coils as close as possible. As a result, the ZCIH technology makes it possible to achieve rapid heating performance with extremely precise exothermic distribution. This paper presents experimental results of a 150-kW six-zone ZCIH system for semiconductor heat processing. © 2010 Wiley Periodicals, Inc. Electr Eng Jpn, 171(1): 37–45, 2010; Published online in Wiley InterScience (
www.interscience. wiley.com ). DOI 10.1002/eej.20908 [ABSTRACT FROM AUTHOR]- Published
- 2010
- Full Text
- View/download PDF
31. Simulation of fiber fuse phenomenon in single-mode optical fibers.
- Author
-
Shuto, Y., Yanagi, S., Asakawa, S., Kobayashi, M., and Nagase, R.
- Abstract
The unsteady-state thermal conduction process in single-mode (SM) optical fiber was studied theoretically with the explicit finite-difference method (FDM). In the numerical calculation it was assumed that the electrical conductivity of the core layer increased rapidly above 1323 K. The core-center temperature changed suddenly and reached over 3×105 K when an optical power of 1 W was input into the core layer heated at 1373 K. This rapid heating of the core initiated the "fiber fuse" phenomenon. The high-temperature core areas, whose radiation spectrum extended over a wide range from the infrared to the ultraviolet regions, were enlarged and propagated toward the light source at a rate of about 0.7 m s-1. This rate was in fair agreement with the experimentally determined value. [ABSTRACT FROM PUBLISHER]
- Published
- 2003
- Full Text
- View/download PDF
32. Effects of induction heat treatment on mechanical properties of TiAl-based alloy.
- Author
-
Peng, Chao-qun, Huang, Bai-yun, and He, Yue-hui
- Abstract
The effects of rapid heating cyclic heat treatment on mechanical properties of a TiAl-based alloy (Ti-33Al-3Cr) were studied by means of an induction heating machine. The results show that: 1) fine fully-lamellar microstructure with colony size of about 50 µm and lamellar spacing of about 0.12 µm can be obtained; 2) the compression mechanical properties can be improved to a large extent and the best comprehensive compression mechanical properties can reach the yield stress 745 MPa, the large flow stress 1 672 MPa and the compression ratio 19.4%; and 3) the compression fracture at room temperature after induction heat treatment and aging is still typical cleavage fracture. [ABSTRACT FROM AUTHOR]
- Published
- 2002
- Full Text
- View/download PDF
33. Ferroelectric properties of modified lead titanate thin films obtained by a sol-gel method.
- Author
-
Carmona, F., Calzada, M., Sirera, R., and Mendiola, J.
- Abstract
Calcium substituted lead titanate thin films have been prepared by a sol-gel method, deposited by spin-coating, and thermally treated so as to obtain a perovskite structure. Two types of thermal treatments were given, differing in the heating rate, which in conventional treatments was of some 10°C/min, and in rapid treatments >500°C/min. With rapid heating, materials are obtained in which greater polarizations are commuted and bias fields are smaller. This, together with the fact that additional (undesired) phases are not observed by X-ray diffractometry when rapid treatments are used, shows that these are to be preferred over conventional treatments. [ABSTRACT FROM AUTHOR]
- Published
- 1997
- Full Text
- View/download PDF
34. Ferroelectric Properties of Modified Lead Titanate Thin Films Obtained by a Sol-Gel Method.
- Author
-
Carmona, F., Calzada, M.L., Sirera, R., and Mendiola, J.
- Abstract
Calcium substituted lead titanate thin films have been prepared by a sol-gel method, deposited by spin-coating, and thermally treated so as to obtain a perovskite structure. Two types of thermal treatments were given, differing in the heating rate, which in conventional treatments was of some 10°C/min, and in rapid treatments > 500°C/min. With rapid heating, materials are obtained in which greater polarizations are commuted and bias fields are smaller. This, together with the fact that additional (undesired) phases are not observed by X-ray diffractometry when rapid treatments are used, shows that these are to be preferred over conventional treatments. [ABSTRACT FROM AUTHOR]
- Published
- 1997
- Full Text
- View/download PDF
35. Rapid Heating in High-Temperature Thermomicroscopic Analysis.
- Author
-
Gibner, Ya. and Vasilyeva, I.
- Abstract
A new technique of rapid heating in high-temperature thermomicroscopic analysis is suggested. The apparatus is described, the metrological features of the method and its advantages and limitations are discussed. Application of the technique to studying the behaviour of refractory Nd
3 S4 , GaP and MoS2 compounds in the temperature range from 25 to 2500°C shown. [ABSTRACT FROM AUTHOR]- Published
- 1998
- Full Text
- View/download PDF
36. High-Temperature Study of Heat-Shielding Composite Materials of the 'Oxide-Oxide' Class.
- Author
-
D'yakonov, V., Lukin, E., Nefedova, N., Pronin, B., and Filatov, E.
- Subjects
THERMAL shielding ,HIGH temperature chemistry ,COMPOSITE materials ,RADIO engineering ,SILICON oxide ,CHEMICAL precursors - Abstract
Results are provided for development and study of radio engineering heat-shielding composite materials. The main properties of composite materials of the SiO-SiO class are demonstrated, and strength and thermophysical properties are determined over the whole working temperature range. Results are presented for a study of improvement of heat-resistant materials of the SiO-SiO class. The effect of refractory oxides ZrO and CrO introduced into the material structure by means of water-soluble precursors on short-term heat resistance is shown. Comparative tests are performed for the original and modified material on heating in a high-temperature gas flame, and the results obtained are evaluated. [ABSTRACT FROM AUTHOR]
- Published
- 2014
- Full Text
- View/download PDF
37. A New Infrared Heat Treatment on Hot Forging 7075 Aluminum Alloy: Microstructure and Mechanical Properties.
- Author
-
Chang, Yi-Ling, Hung, Fei-Yi, and Lui, Truan-Sheng
- Subjects
HEAT treatment ,ALUMINUM alloys ,MECHANICAL alloying ,MECHANICAL properties of condensed matter ,FORGING ,PRECIPITATION hardening - Abstract
When hot forging 7075 aluminum alloy, as a military material durable enough for most of its applications, it needs to be heat-treated to ensure the target material property achieves the application requirements. However, the material properties change because of heat throughout usage. In this study, a new approach was devised to heat treat the alloy to prevent material property changes. The study further clarified the effect of rapid heat treatment on the high-temperature resistance of a hot forging 7075 aluminum alloy. Infrared (IR) heat treatment was used as a rapid heating technique to effectively replace the conventional resistance heat (RH) treatment method. Our experimental result showed that IR heat treatment resulted in better age hardening at the initial aging stage, where its tensile strength and elongation appeared like that of a resistance heat treatment. More so, based on hardness and tensile test results, the IR-heated treatment process inhibited the phase transformation of precipitations at a higher temperature, improving high-temperature softening resistance and enhancing the thermal stability of the hot forging 7075 aluminum alloy. [ABSTRACT FROM AUTHOR]
- Published
- 2020
- Full Text
- View/download PDF
38. Lethal Effects of High Temperatures on Brown Marmorated Stink Bug Adults before and after Overwintering.
- Author
-
Scaccini, Davide, Duso, Carlo, and Pozzebon, Alberto
- Subjects
BROWN marmorated stink bug ,HIGH temperatures ,ADULT day care ,TEMPERATURE effect ,HEAT treatment ,ADULTS - Abstract
The invasive brown marmorated stink bug, Halyomorpha halys, is causing economic and ecological damage in invaded areas. Its overwintering behavior warrants mitigation practices in warehouses and shipping operations. The aim of this study was to characterize the mortality response curves of H. halys adults to short high-temperature exposure. Here we compared field-collected individuals entering (ENA) and exiting diapause (EXA). EXA adults displayed increased susceptibility to high temperatures compared to ENA individuals. Complete mortality of all tested individuals was obtained after 10 min exposure at 50.0 °C, and after 15 (EXA) or 20 min (ENA) at 47.5 °C. The nutritional status of these insects had no effect on high-temperature tolerance. The mortality curves obtained here may be used for the definition of cost-effective heat treatments aimed at the H. halys control. [ABSTRACT FROM AUTHOR]
- Published
- 2019
- Full Text
- View/download PDF
39. A Rapid Thermal Nanoimprint Apparatus through Induction Heating of Nickel Mold.
- Author
-
Fu, Xinxin, Chen, Qian, Chen, Xinyu, Zhang, Liang, Yang, Aibin, Cui, Yushuang, Yuan, Changsheng, and Ge, Haixiong
- Subjects
NANOIMPRINT lithography ,NICKEL ,INDUCTION heating ,MAGNETIC flux leakage ,SPECIFIC heat ,FERROMAGNETIC materials ,MAGNETIC hysteresis - Abstract
Thermal nanoimprint lithography is playing a vital role in fabricating micro/nanostructures on polymer materials by the advantages of low cost, high throughput, and high resolution. However, a typical thermal nanoimprint process usually takes tens of minutes due to the relatively low heating and cooling rate in the thermal imprint cycle. In this study, we developed an induction heating apparatus for the thermal imprint with a mold made of ferromagnetic material, nickel. By applying an external high-frequency alternating magnetic field, heat was generated by the eddy currents and magnetic hysteresis losses of the ferromagnetic nickel mold at high speed. Once the external alternating magnetic field was cut off, the system would cool down fast owe to the small thermal capacity of the nickel mold; thus, providing a high heating and cooling rate for the thermal nanoimprint process. In this paper, nanostructures were successfully replicated onto polymer sheets with the scale of 4-inch diameter within 5 min. [ABSTRACT FROM AUTHOR]
- Published
- 2019
- Full Text
- View/download PDF
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