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1. An alternative synthesis of 2,6-dimethoxyl-1,4-benzoquinone.

Author

Qian Wang, Jian Yang, Yang Zheng, and Xiali Liao

Subjects
METABOLITE synthesis, ANILINE, DEAMINATION, CHEMICAL yield, CHEMICAL reactions
Abstract

An economic four-step synthesis of 2,6-dimethoxy-1,4-benzoquinone was achieved in 68 % overall yield starting from aniline. The reaction sequence involved conversion to1,3,5-tribromoaniline, deamination, methoxylation, and oxidation. The procedure is operationally simple and amenable to scale-up production. [ABSTRACT FROM AUTHOR]

Published
2017
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