1. Synthesis, Characterization, Optical Properties, and Electron Paramagnetic Resonance for Nano ZnCoFePr O.
- Author
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Bitar, Z., Isber, S., Noureddine, S., Bakeer, D., and Awad, R.
- Subjects
X-ray diffraction ,FERRITES ,COPRECIPITATION (Chemistry) ,TRANSMISSION electron microscopes ,MAGNETIC fluids - Abstract
Nano ferrite samples of type ZnCoFe Pr O , 0 ≤ x ≤ 0.2, were prepared by co-precipitation method for different concentration of Pr ions at a calcination temperature of 823 K. The samples were characterized using x-ray diffraction and transmission electron microscope (TEM), UV spectroscopy, FTIR, and electron paramagnetic resonance (EPR). The increase in concentration of Pr ions shows a significant change in the formed nano ferrite particles size, degree of aggregation, energy band gap, and lattice parameters. X-band (9.24 GHz) EPR spectra at room temperature showed a decrease in the g factor as the Pr content was increased. Furthermore, the variation of the Pr concentration in the samples led to different aggregation states, ranging from isolated nanoparticles with average crystal size of 28.5 to about 15 nm, as confirmed by x-ray diffraction and high-resolution transmission electron microscopy. [ABSTRACT FROM AUTHOR]
- Published
- 2017
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