1. Assessing the experimental investigation of milk thistle oil for biodiesel production using base catalyzed transesterification.
- Author
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Ullah, Kifayat, Ahmad, Mushtaq, Sofia, null, and Qiu, Fengxian
- Subjects
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MILK thistle , *BIODIESEL fuels , *VEGETABLE oils as fuel , *BIOMASS production , *TRANSESTERIFICATION , *CHEMICAL synthesis , *ESTERIFICATION - Abstract
In the present research work, non edible oil source milk thistle ( Silybum marianum (L.) Gaert) plant was investigated for biodiesel production. The extracted crude oil was 26.14% of the total seed dry weight. The free fatty acid content of oil was reduced from 0.56 mg KOH/g to 0.06 mg KOH/g by esterification before the synthesis of biodiesel. The highest conversion percentage of biodiesel was achieved 89.51% and 87.42% using solid base catalyst sodium hydroxide (0.75%) and potassium hydroxide (1.0%), respectively. The protocol for experiment was adjusted as follow: temperature (60 °C); time of reaction (2 h), steering (600 rpm) and the oil molar ratio was fixed 1:6. Qualitatively, the prepared biodiesel was quantified by GC chromatography, 13 C & 1 H NMR (Nuclear Magnetic Resonance), AAS and FT-IR spectroscopy. The fuel properties of biodiesel were tested and compared with ASTM D6751 and EN 14214 standards. [ABSTRACT FROM AUTHOR]
- Published
- 2015
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