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Despite its relevance for law enforcement applications, the design of soft armor has mainly been based on a trial-and-error approach. In this paper, a combined experimental, machine learning, and finite element analysis framework is used to build a predictive numerical model for the analysis and hence, design of soft armor. The material models for major components of the soft armor certification system--bullet, shoot pack, straps, and clay backing, are first constructed using laboratory tests and publicly available data. Next, three metrics, namely, back face signature (BFS), number of penetrated shoot-pack layers, and mushrooming of the bullet are established to gauge the model's accuracy with respect to the laboratory ballistic test data. A machine learning (ML) model is used as a surrogate to predict the BFS and the number of eroded elements. Finally, optimized material model parameters are obtained through ML-based surrogate model and Bayesian optimization algorithm. The final validation of the developed framework is carried out using laboratory ballistic test data involving multiple shots on the shoot pack. The results indicate that reliable predictive data can be obtained using the developed process, and likely, can be extended for use in modeling other impact simulations. [ABSTRACT FROM AUTHOR]

In the present research, glass and basalt fiber-reinforced polypropylene composites' behaviour in quasi-static and dynamic conditions is studied. Composites were fabricated by vacuum assisted Compression molding method. Composites failure under quasi-static tension and compressive conditions was studied along with its failure behaviour under low-velocity impact and super-sonic shock loading under dynamic conditions. The study results showed that basalt fiber-reinforced polypropylene (Basalt/PP) composite's tensile and compressive strength is higher than glass fiber-reinforced polypropylene (Glass/PP). The Basalt/PP showed no penetration against low velocity impact (LVI) with negligible deformations till 50 J. However, the Glass/PP perforated at 50 J with various failure patterns occurring at back side. The fiber-matrix interface adhesion plays an important role in super-sonic shock loading by absorbing shock wave energy due to ductile nature of polypropylene and the two composites absorbed energy via matrix and fibers failure, no brittle failure of laminates occurred under shock loading. [ABSTRACT FROM AUTHOR]

All bioresorbable polymeric implants are radiolucent, making them undetectable under the X-rays. Therefore, to improve their X-ray visibility, the high effective atomic number (Zeff) material such as Pt, Au, Ta, Ba, or its alloy are attached to the body of the bioresorbable implant. However, during the in vivo degradation, these bio-inert heavy metals can either detach or leach out from the lesion site and accumulate into the vital organ, leading to severe health complications. Thus, as a strategy, the novel biodegradable and radiopaque Mg alloy was produced to impart X-ray visibility in the biopolymer. Here, the Mg was alloyed with the optimized ratio of heavy metals, i.e., Zn and Y. The radiopaque Mg alloy was characterized and powdered to the size of 25–20 µm. Further, it was blended with radiolucent Poly-L-lactic acid (PLLA) and polycaprolactone (PCL) polymer. The Bi-axially expanded (BAE) tubes of PLLA/PCL and PLLA/PCL/Mg alloy (5% wt.) were extruded for fabricating cardiovascular stents. The BAE tube comparison studies were performed for thermal stability, wettability, surface roughness, and mechanical properties. The potential of 5% Mg alloy in the polymeric matrix was evaluated as a nucleating, reinforcing, and radiopaque agent. In vitro accelerated degradation study was performed in the physiological fluid to evaluate the pH variation and decomposition rate. Finally, in vitro biocompatibility was assessed by evaluating the behavior of L929 fibroblast cells, followed by the blood biocompatibility test on the blends. [ABSTRACT FROM AUTHOR]

In this study, the effect of high strain rate on the dynamic mechanical properties of shear thickening fluid (STF) impregnated felt of ultra‐high molecular weight polyethylene (UHMWPE) was investigated by split‐hopkinson pressure bar. UHMWPE felts are randomly oriented nonwoven fabric that holds each other due to inter‐fiber coupling either by thermal calendaring or mechanical entanglement. Its lower areal density and highly porous structure can be utilized in lightweight ballistic resistance material. The junction points inside its porous structure make it easier to hold abundant STF. Shear thickening fluid was prepared by dispersing 100 nm dry silica powder into polypropylene glycol at 67.5 wt% concentration using probe ultrasonicator at 25°C. Rheological characterization of prepared STF was conducted using MCR702 advanced Anton Paar rheometer. It was done by performing a steady shear rate and thixotropy tests for shear thickening and structural regeneration behavior. In‐house fabricated split‐hopkinson pressure bar setup was used to evaluate dynamic compressive behavior at different strain rates by changing triggering pressure. It was found that STF impregnated felt shows a higher amplitude of strain rate augmentation and energy absorption than a neat felt. The impact energy absorption increases with increasing strain rate. However, the peak stress shows an opposite trend with an increased strain rate in STF impregnated felt. [ABSTRACT FROM AUTHOR]

Compressive behaviour of open and closed cell polyurethane foam samples under large deformation is studied using micro‐Computed Tomography (micro‐CT), Digital Volume Correlation (DVC) technique and micro‐Finite Element (micro‐FE) modelling. The micro‐CT images of the foam samples at different compression strains are used to determine anisotropy in the foams, to obtain qualitative information on deformation mechanisms, to quantify the deformation and strains using a local DVC approach and to generate images for micro‐FE modelling of the foam samples. Micro‐FE modelling predicts the deformation using an elastoplastic material model coupled with continuum damage mechanics. Two different types of boundary conditions, experimentally derived (ExBC) and interpolated from DVC (IPBC), were implemented to evaluate the displacements in the micro‐FE models. A reduced integration scheme in micro‐FE analysis resulted in high artificial energy and was discarded in favour of full integration. The displacement predicted by IPBC matched with DVC displacement contours for closed cell foam. The ExBC‐predicted axial displacement (W) showed a better agreement with DVC than transverse displacements (U, V) contours. However, a significant statistical comparison (R2 > 0.70) of all displacements was obtained for both IPBC and ExBC. For open cell foam, both boundary conditions predicted a significant difference in the displacement contours with respect to DVC measurements. Still, the axial displacements of ExBC and IPBC showed a better statistical significance (R2 > 0.70). [ABSTRACT FROM AUTHOR]

PLA and its blends are the most extensively used materials for various biomedical applications such as scaffolds, implants, and other medical devices. The most extensively used method for tubular scaffold fabrication is by using the extrusion process. However, PLA scaffolds show limitations such as low mechanical strength as compared to metallic scaffolds and inferior bioactivities, limiting their clinical application. Thus, in order to improve the mechanical properties of tubular scaffolds, they were biaxially expanded, wherein the bioactivity can be improved by surface modifications using UV treatment. However, detailed studies are needed to study the effect of UV irradiation on the surface properties of biaxially expanded scaffolds. In this work, tubular scaffolds were fabricated using a novel single-step biaxial expansion process, and the surface properties of the tubular scaffolds after different durations of UV irradiation were evaluated. The results show that changes in the surface wettability of scaffolds were observed after 2 min of UV exposure, and wettability increased with the increased duration of UV exposure. FTIR and XPS results were in conjunction and showed the formation of oxygen-rich functional groups with the increased UV irradiation of the surface. AFM showed increased surface roughness with the increase in UV duration. However, it was observed that scaffold crystallinity first increased and then decreased with the UV exposure. This study provides a new and detailed insight into the surface modification of the PLA scaffolds using UV exposure. [ABSTRACT FROM AUTHOR]

Material systems capable of handling both the ballistic impact and blast waves are necessary for security forces. In this study, the high strain rate performance of monolithic and bonded ultra‐high molecular weight polyethylene (UHMWPE) with high‐temperature resistant basalt/polyetherimide (B/PEI) composite is presented. Individual composite laminates were fabricated using vacuum‐assisted compression molding. Subsequently, cylindrical test coupons were cut using a high‐pressure waterjet. A suitable adhesive grade was used for the bonding of two different composite types. The dynamic compression studies were conducted on a split‐Hopkinson pressure bar (SHPB). For identical incident energies, the range of strain rates attained by monolithic UHMWPE, B/PEI and bonded composites differed significantly. Monolithic UHMWPE achieved the highest rates of loading, whereas higher stresses were recorded for the B/PEI composite. Yet, monolithic UHMWPE, owing to higher constant stress plastic flow, results in higher toughness. Bonded composites revealed hybrid properties with delamination of UHMWPE as the primary failure mode. High‐speed imaging exposed severe deformation of UHMWPE during dynamic compression. SEM micrographs revealed fiber pull‐out and deforming behavior of UHMWPE and brittle failure of B/PEI composite. B/PEI in a bonded composite system never failed under dynamic compression within the experimental range, thus providing a window of opportunity to tailor‐make better ballistic and blast protection materials. [ABSTRACT FROM AUTHOR]

An investigation of the effect of strain rate on the dynamic compressive behavior of glass/polytetrafluoroethylene (PTFE) composite is presented. Experimental studies were carried out on two dimensional (2D), satin weave (SW) and three dimensional (3D) woven glass/PTFE composites using split Hopkinson pressure bar (SHPB) apparatus. Commercial grades of glass/PTFE fabrics were autoclaved to prepare the composite laminates and circular specimens were cut out using a high‐pressure water jet. High strain rate studies confirmed the rate‐dependent behavior of all the woven composite systems under consideration. The highest rates of loading were attained by 3D woven specimens for identical incident energies. The highest peak stress attained by 3D woven specimens was 501 MPa, which was trailed by 2D woven specimens with 482 MPa stress. The advantage of satin weave was not reflected in the small specimens as the peak stress attained for identical loading was limited to 405 MPa. Similarly, the highest strain and toughness were recorded for 3D woven composites. However, the SW pattern unlocked a new possibility of controlling the primary damage axis. Furthermore, an analytical method is presented based on variable rate power law to predict the dynamic compressive stress of glass/PTFE. [ABSTRACT FROM AUTHOR]

The surface of dental implants plays a vital role in early and more predictable osseointegration. SLA (sandblasted large grit and acid-etched) represents the most widely accepted, long-term clinically proven surface. Primarily, dental implants are manufactured by either commercially pure titanium (CP-Ti) or Ti6Al4V ELI alloy. The acid etch behavior of CP-Ti is well known and its effects on the surface microstructure and physicochemical properties have been studied by various researchers in the past. However, there is a lack of studies showing the effect of acid etching parameters on the Ti6Al4V alloy surface. The requirement of the narrow diameter implants necessitates implant manufacturing from alloys due to their high mechanical properties. Hence, it is necessary to have an insight on the behavior of acid etching of the alloy surface as it might be different due to changed compositions and microstructure, which can further influence the osseointegration process. The present research was carried out to study the effect of acid etching parameters on Ti6Al4V ELI alloy surface properties and the optimization of process parameters to produce micro- and nanotopography on the dental implant surface. This study shows that the Ti6Al4V ELI alloy depicts an entirely different surface topography compared to CP-Ti. Moreover, the surface topography of the Ti6Al4V ELI alloy was also different when etching was done at room temperature compared to high temperature, which in turn affected the behavior of the cell on these surfaces. Both microns and nano-level topography were achieved through the optimized parameters of acid etching on Ti6Al4V ELI alloy dental implant surface along with improved roughness, hydrophilicity, and enhanced cytocompatibility. [ABSTRACT FROM AUTHOR]

The dynamic behaviour of the High Strength Low Alloy (HSLA) Steel before and after heat treatment was examined experimentally by performing quasi-static and high strain rate testing at room temperature and cryogenic temperatures. The high strain rate tensile testing of the material was performed on a Split Hopkinson Tensile Bar (SHTB) setup. A customized liquid nitrogen chamber equipped with UTM and SHTB was used to perform the cryogenic temperature testing. The stress–strain response of the material under different loading conditions was recorded and a modified Johnson–Cook material model was derived. It was observed that the flow stress of the material increased when tested at a high strain rate and it further increased at a cryogenic high strain rate loading environment. The microstructure of the material before and after heat treatment was also observed to identify the dominant phase change in microstructure contributing towards improvement in strength after heat treatment. The failure analysis of each category of the samples was examined under the Scanning Electron Microscope (SEM) after the testing. The formation of small and deep dimples for as-received samples and bigger and shallow dimples for heat-treated samples distinguished the type of failure between the quasi-static, high strain rate and cryogenic high strain rate material testing. • High Strength Low Alloy Steel (HSLA) were characterized at Quasi-Static and high strain rate tensile testing at room temperature and cryogenic temperature in both annealed and post heat treated conditions. • The customized Split Hopkinson Tensile Bar equipped with liquid nitrogen chamber and on-board temperature measurement system was developed to perform high strain rate cryogenic testing of HSLA steel. • The fractured surface of annealed and post heat treated samples were examined to understand the underlying effect contributing towards improvement in mechanical properties of the HSLA steel. • The modified Johnson–Cook material model parameters were derived based on the experimental results. The numerical simulations were performed to verify the developed constituent model. [ABSTRACT FROM AUTHOR]

• High hardness steel (HHS) sheet with UHMWPE composite backing were tested against a hardened steel core projectile. • The projectile core was eroded by the HHS sheet and stopped in UHMWPE composite. • It is observed that only a core eroded to a certain length and weight by armor system can be defeated. • In numerical modeling core failure strain was determined from the residual weight of cores. • The numerical model can be used to evolve armor design. Thin high hardness steel sheets can be an alternative to expensive ceramic armor systems designed to defeat hardened core projectiles. A thin high hardness steel sheet backed with UHMWPE fiber-reinforced composite was ballistically tested against a 7.62 × 39 mm hardened steel core projectile in a single-stage gas gun. Thin steel sheets of 530 BHN hardness were adhesively bonded with UHMWPE fiber-reinforced composite to fabricate armor plates. Armor plates were able to defeat the projectile showing considerable potential. Tensile strength of steel sheet and UHMWPE-fiber reinforced ply was also determined. A detailed numerical simulation of the impact event was also performed to understand the phenomenon of defeat and penetration in greater detail. The numerical model was calibrated from the recovered projectile's core after the ballistic test. [ABSTRACT FROM AUTHOR]

• Vacuum compression moulded Basalt-Polyeteherimide (PEI) composites manufacturing. • Optimization of Basalt-PEI composite manufacturing moulding parameters. • Basalt-PEI composite under quasi-static and dynamic high strain rate loading. • Elastic recovery of Basalt-PEI composite can help in reflecting the blast wave. High temperature blast and ballistic resistant light weight fibre reinforced plastic composites are very much in demand. Accordingly, the present investigation is focused on the quasi-static and high strain rate behaviour of Basalt/Polyetherimide (PEI) composite. Nine different types of composite samples were fabricated by compression moulding. The moulding pressures and temperatures were varied in the range of 15–25 bars and 325 °C−375 °C, respectively. Quasi-static testing was done at the rate of 3 mm/min to establish the optimum moulding parameters. High strain rate compression tests in the strain rate range of 900/s−3200/s were performed on the optimum moulded composite specimens. High strain rate testing revealed that 40 layered Basalt/PEI composite moulded at 25 bar pressure and 350 °C attained highest stress of 932 MPa whereas, the same was found to attain 446 MPa under quasi-static loading conditons. Thus, establishing the rate depedency of Basalt/PEI composite. Damage studies revealed that Basalt/PEI undergoes brittle damage, typically resulting in shear plane angle of 42°−45°. SEM micrographs revealed brittle fibre failure and matrix free fibre bundles, indicating the importance of process parameter optimiation. [ABSTRACT FROM AUTHOR]