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1. Interaction of 2,4,6-tris(2-pyrimidyl)-1,3,5-triazine (TPymT) with CoX2 (X = Cl, Br) in water: trapping of new self-assembled water–chloride/bromide clusters in a [Co(bpca)2]+ host (bpca = bis(2-pyrimidylcarbonyl)amidate anion)

Author

Safin, Damir A., Szell, Patrick M. J., Keller, Antonin, Korobkov, Ilia, Bryce, David L., and Murugesu, Muralee

Subjects
*CHLORIDES, *BROMIDES, *POLYMERIC composites, *MAGNETIC resonance, *SPECTRUM analysis
Abstract

2D polymeric water–chloride/bromide sheets comprising a unique pentagon-like dichloride/dibromide-trihydrate cluster in the solid state have been observed as [Co(bpca)2]+ (bpca = bis(2-pyrimidylcarbonyl)amidate anion) counterions. Both compounds were obtained by the reaction of 2,4,6-tris(2-pyrimidyl)-1,3,5-triazine (TPymT) with CoX2 (X = Cl, Br) in water. Solid-state multinuclear magnetic resonance spectroscopy and XRD provide insight into the structures. [ABSTRACT FROM AUTHOR]

Published
2015
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