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1. Characterization and Crystal Structure of a Novel Mononuclear Cobalt(II) Complex with Hydrazone Derived from Protocatechuic Acid.

Author

Sheng, G.-H., Wang, C.-F., Feng, S., Gao, X., and Zhu, H.-L.

Subjects
*CRYSTAL structure, *COBALT, *HYDRAZONE derivatives, *MONOCLINIC crystal system, *UNIT cell
Abstract

A novel complex [CoII(L)2·CH3OH] with hydrazone derived from protocatechuic acid (HL=C16H14N2O4) is designed and synthesized. The complex is characterized by single crystal X-ray diffraction, elemental analysis, IR, and thermal gravimetric analysis. The complex crystallizes in the monoclinic space group C2/c, with unit cell dimensions a = 25.1715(11), b = 9.3518(4), c = 12.8700(6) Å, β = 103.6530(10)°, V = 2943.98(75) Å3, Z = 4, R1 = 0.0612, and wR2 = 0.1439. [ABSTRACT FROM AUTHOR]

Published
2018
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