1. A Green Approach for the Synthesis of Silver Nanoparticles Using Ultrasonic Radiation’s Times in Sodium Alginate Media: Characterization and Antibacterial Evaluation.
- Author
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Faried, Miftah, Shameli, Kamyar, Miyake, Mikio, Hajalilou, Abdollah, Zamanian, Ali, Zakaria, Zuriati, Abouzari-lotf, Ebrahim, Hara, Hirofumi, Ahmad Khairudin, Nurul Bahiyah Bt, and Binti Mad Nordin, Mariam Firdhaus
- Subjects
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SILVER nanoparticles , *NANOSTRUCTURED materials synthesis , *SODIUM alginate , *ULTRASONIC waves , *ANTIBACTERIAL agents , *SUSTAINABLE chemistry , *X-ray diffraction - Abstract
The synthesis of silver nanoparticles (Ag-NPs) was achieved by a simple green chemistry procedure using sodium alginate (Na-Alg) under ultrasonic radiation as a stabilizer and physical reducing agent. The effect of radiation time on the synthesis of Ag-NPs was carried out at room temperature until 720 min. The successful formation of Ag-NPs has been confirmed by UV-Vis, XRD, TEM, FESEM-EDX, zeta potential, and FT-IR analyses. The surface plasmon resonance band appeared at the range of 452–465 nm that is an evidence of formation of Ag-NPs. The XRD study showed that the particles are crystalline structure in nature, with a face-centered cubic (fcc) structure. The TEM study showed the Ag-NPs have average diameters of around 20.16–22.38 nm with spherical shape. The FESEM-EDX analysis confirmed the spherical shape of Ag-NPs on the surface of Alg and the element of Ag with the high purity. The zeta potential showed high stability of Alg/Ag-NPs especially after 720 min irradiation with value of −67.56 mV. The FT-IR spectrum confirmed that the Ag-NPs have been capped by the Alg with van der Waals interaction. The Alg/Ag-NPs showed the antibacterial activity against Gram-positive and Gram-negative bacteria. These suggest that Ag-NPs can be employed as an effective bacteria inhibitor and can be applied in medical field. [ABSTRACT FROM AUTHOR]
- Published
- 2016
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