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2. Molecular simulation of different types of polysilsesquioxane doped cellulose insulating paper: A guide for special cellulose insulating paper.
- Author
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Zeng, Zhenglin, Tan, Weimin, Deng, Yanhe, Cheng, Quan, Fu, Liuyue, and Tang, Chao
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CELLULOSE fibers , *CELLULOSE , *GLASS transition temperature , *MODULUS of rigidity , *BULK modulus , *ELASTIC modulus , *DIELECTRIC properties - Abstract
To develop special insulating paper is of great significance to promote the service life of transformers. Using molecular simulation to guide the development of special insulating paper can greatly reduce the trial-and-error rate and waste of resources in traditional experiments. The effect of different types of polysilsesquioxane (POSS) on cellulose insulating paper was investigated by using molecular simulation. This paper investigated the thermal stability and mechanical properties and electrical characteristics of caged POSS, semi-caged POSS, and ladder-like POSS doped cellulose insulating paper. The results show that POSS with all types can enhance the performance of cellulose insulating paper, and ladder-like POSS possess the best modification effect. The glass transition temperature was increased by 58 K, and the bulk modulus, shear modulus, and elastic modulus of cellulose insulating paper doped with ladder-like POSS can improve up to 27.07%, 45.67%, and 41.28%, respectively. Meanwhile, the dielectric properties of ladder-like POSS modified insulating paper are also significantly improved. The findings of this paper propose a method for the preparation of ladder-like POSS modified insulating paper, which provides theoretical guidance for the experimental preparation of special insulating paper. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
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3. Fabrication of negative magnetostrictive Japanese traditional paper (washi) with cobalt ferrite particles.
- Author
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Kurita, Hiroki, Rova, Lovisa, Keino, Takumi, and Narita, Fumio
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MAGNETOSTRICTION , *FERRITES , *COBALT , *JAPANESE language , *WOOD-pulp , *CELLULOSE fibers , *MAGNETIC particles - Abstract
The cellulose fibers that form washi are longer than those of regular paper made from wood pulp. Hence, the mechanical properties of washi can be higher than those of conventional paper. This study evaluated the magnetic, magnetostrictive, and tensile properties of negative magnetostrictive cobalt ferrite (CoFe2O4) particle dispersed handmade washi (washi−CoFe2O4). The CoFe2O4 additives magnetized the washi, which displayed negative magnetostriction with the fiber direction perpendicular to the magnetic field and in the parallel fiber direction. Concerning the mechanical properties, the washi−CoFe2O4 displayed an elongation of up to 77% after yielding. [ABSTRACT FROM AUTHOR]
- Published
- 2023
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4. Reactive molecular dynamics research on influences of water on aging characteristics of PMIA insulation paper.
- Author
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Wang, Lihan, Yin, Fei, Shen, Yin, and Tang, Chao
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MOLECULAR dynamics , *INSULATING oils , *CHEMICAL stability , *HYDROXYL group , *ACTIVATION energy , *MOISTURE content of food - Abstract
The diffusion of moisture in the meta-aramid fiber (PMIA) oil-paper insulation system and the thermal decomposition of PMIA insulation paper in different moisture contents were studied via molecular dynamics simulations. The results showed that the PMIA insulation paper had a stronger ability to absorb water molecules than the insulating oil; therefore, water molecules in the insulating oil diffuse to the insulation paper, which further affects the thermal decomposition of the PMIA insulation paper. The activation energy of the water-bearing composite model was 129.96 kJ/mol, which was 5.5% lower than that of the pure PMIA (137.61 kJ/mol). It indicated that moisture could promote PMIA decomposition. The micromechanism of the enhanced thermal decomposition of PMIA with moisture contents could be described as follows: The O–H bond of the water can easily break to generate H atoms and hydroxyl radicals (•OH). The strong activity of H atoms allows it to easily combine with the ammonia base at the end of PMIA to generate NH3. Additionally, the free •OH radical can easily combine with the amido and carbonyl bonds at two ends of PMIA, undergo an oxidation reaction, and generate an oxhydryl. Therefore, it can reduce the chemical stability of the PMIA chain and further drive thermal decomposition. Statistical data on fragments generated by the thermal decomposition of the water-bearing PMIA composite system show that the main products include H2, C/H/O-containing molecules, hydrocarbon molecules, N-bearing molecules, and free radicals. [ABSTRACT FROM AUTHOR]
- Published
- 2020
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5. Fabrication and characterization of graphene-based paper for heat spreader applications.
- Author
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Muhsan, Ali A. and Lafdi, Khalid
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THERMAL conductivity measurement , *THERMAL conductivity , *CHEMICAL processes , *CHEMICAL vapor deposition , *SCANNING electron microscopy , *SLURRY - Abstract
In this work, in-plane thermal conductivity measurement was carried out on graphene-based papers. Graphene-based papers were fabricated using various processing techniques such as chemical vapor deposition (CVD), hot pressing of graphene slurry, and evaporation induced self-assembly. The prepared materials were characterized using scanning electron microscopy, Raman spectroscopy, and X-ray diffraction. In-plane thermal conductivity measurement was performed via a steady state thin film thermal conductivity apparatus. The in-plane thermal conductivity measurements show that the CVD based sample has the highest thermal conductivity. COMSOL Multiphysics was used to simulate the in-plane thermal conductivity of graphene-based papers. [ABSTRACT FROM AUTHOR]
- Published
- 2019
- Full Text
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6. Improvements of mechanical properties of multilayer open-hole graphene papers.
- Author
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Xia, Yuxuan, Li, Yeyuan, Zhu, Chunhua, Wei, Ning, and Zhao, Junhua
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SHEAR strength , *CARBON-carbon bonds , *TENSILE strength , *STRESS concentration , *COVALENT bonds , *LAMINATED glass - Abstract
Holes and defects can greatly reduce the mechanical properties of multilayer graphene sheets under different loading conditions due to the stress concentration near the hole edge in each in-plane sheet and the lack of interlayer carbon–carbon bonds between the layers. Here, we report a novel design of multilayer open-hole graphene papers (MLGPs) formed through interlayer covalent bonding at the hole edges of multilayer open-hole graphene sheets (MLGSs) under high temperature using molecular dynamics (MD) simulations. Our MD results show that the hybrid sp2–sp3 interlayer bonds of MLGPs can significantly improve their both tensile strength and interlayer shear strength. The tensile strength and interlayer shear strength of MLGPs increase by around 20% and 3 times by comparison with those of MLGSs with the same number of layers, respectively, which mainly depends on the uniformity of their interlayer bond distribution. This study can provide an effective way to improve the mechanical performances of multilayer graphene sheets with flaws and also offer corresponding guidance for the design of MLGS-based nanocomposites. [ABSTRACT FROM AUTHOR]
- Published
- 2019
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7. Negative elastic wave refraction and focusing regulation of single-phase solid phononic crystals.
- Author
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Liu, Fei-Yu, Wang, Fa-Jie, and Zhao, Sheng-Dong
- Subjects
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ELASTIC waves , *PHONONIC crystals , *NEGATIVE refraction , *LONGITUDINAL waves , *DISTRIBUTION (Probability theory) , *SHEAR waves - Abstract
This paper presents the design of a single-phase solid phononic crystal (PnC) structure featuring a regular hexagonal perforation pattern. The structure manifests three negative refraction bands, encompassing one for transverse waves and two for longitudinal waves, thereby enabling simultaneous control of shear and longitudinal waves. Due to the high symmetry of the triangular lattice, the equal frequency curves corresponding to the negative refraction band approach circular shapes, suggesting a nearly isotropic negative refraction effect. This negative refraction effect is achieved through specific mass resonance modes closely related to the porous structure designed in this paper. Initially, we analyze the band structure of the PnC, followed by designing the PnC plate structure to achieve negative refraction control for transverse waves at a frequency of 32.4 kHz, with a negative refraction index of −1. Additionally, negative refraction control for longitudinal waves is attained at frequencies of 44 and 64.54 kHz. Subsequently, we scrutinize the influence of various conditions on negative refraction, including different structural parameters, incident angles, and operating frequencies, while verifying the robustness of the designed phonon crystal structure. Leveraging the negative refraction characteristics of the structure, we construct an elastic wave lens to achieve perfect imaging of shear and longitudinal waves. Finally, employing finite element simulation and analyzing focusing imaging characteristics with different source positions, we validate that the results closely align with theoretical expectations. The solid PnC structure designed in this study holds significant potential for applications in the fields of elastic wave imaging. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
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8. A programmable metasurface based on acoustic black hole for real-time control of flexural waves.
- Author
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Su, Kun and Li, Lixia
- Subjects
- *
FREQUENCY changers , *REAL-time control , *ELASTIC waves , *STRUCTURAL engineering , *ACTIVE medium , *SOLAR atmosphere , *SMART structures - Abstract
The time-modulated active medium with linear independent frequency conversion method has been demonstrated to enable wave orientation and reconstruction. However, due to the symmetric scattering field, this technique requires intricate microcircuit designs. To overcome this limitation, this paper proposes a tunable piezoelectric metasurface based on acoustic black holes (ABHs) to redirect flexural wave reflections. The system can convert an incident flexural wave into a reflected wave of any direction and frequency. This is accomplished through the linear time modulation of the sensing signal, which breaks the constraints of Snell's law inherent in traditional designs and is insensitive to the incident amplitude. The coupling of the ABH damping system with a linear independent frequency conversion mechanism allows for the conversion of an incident flexural wave into a reflected wave in any direction and frequency while also eliminating the influence of second harmonic reflection on the wave field and simplifying the time modulation circuit. In addition, this paper demonstrates arbitrary angle reflection, focusing, beam splitting, and frequency conversion of the incident wave. By improving the flexibility of elastic wave manipulation, this paper introduces a new approach for active control of elastic waves and provides a design method that can be employed in a variety of applications ranging from vibration protection of engineering structures to vibration sensing and evaluation. [ABSTRACT FROM AUTHOR]
- Published
- 2024
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9. Electrically and magnetically dual-driven Janus particles for handwriting-enabled electronic paper.
- Author
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Komazaki, Y., Hirama, H., and Torii, T.
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JANUS particles , *ELECTRONIC paper , *MICROFLUIDIC analytical techniques , *SUPERPARAMAGNETIC materials , *NANOPARTICLES , *ELECTRIC potential , *MAGNETIC fields , *INTERNET forums - Abstract
In this work, we describe the synthesis of novel electrically and magnetically dual-driven Janus particles for a handwriting-enabled twisting ball display via the microfluidic technique. One hemisphere of the Janus particles contains a charge control agent, which allows the display color to be controlled by applying a voltage and superparamagnetic nanoparticles, allows handwriting by applying a magnetic field to the display. We fabricated a twisting ball display utilizing these Janus particles and tested the electric color control and handwriting using a magnet. As a result, the display was capable of permitting handwriting with a small magnet in addition to conventional color control using an applied voltage (80 V). Handwriting performance was improved by increasing the concentration of superparamagnetic nanoparticles and was determined to be possible even when 80V was applied across the electrodes for 4 wt.% superparamagnetic nanoparticles in one hemisphere. This improvement was impossible when the concentration was reduced to 2 wt.% superparamagnetic nanoparticles. The technology presented in our work can be applied to low-cost, lightweight, highly visible, and energy-saving electronic message boards and large whiteboards because the large-size display can be fabricated easily due to its simple structure. [ABSTRACT FROM AUTHOR]
- Published
- 2015
- Full Text
- View/download PDF
10. Understanding ac losses in CORC cables of YBCO superconducting tapes by numerical simulations.
- Author
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Nguyen, Linh N., Shields, Nathaniel, Ashworth, Stephen, and Nguyen, Doan N.
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SUPERCONDUCTING coils , *SUPERCONDUCTING cables , *HIGH temperature superconductors , *CABLES , *FINITE element method , *COMPUTER simulation , *ADHESIVE tape , *CURRENT distribution - Abstract
Alternating current (ac) losses in conductor-on-rounded-core (CORC) cables of YBCO high-temperature superconducting (HTS) tapes are a significant challenge in HTS power applications. This study employs two finite element analysis (FEA) models to investigate the contributions from different ac loss components and provide approaches for reducing ac losses in cables. An FEA model based on the T-A formulation treats the cross section of thin superconducting layers as 1D lines and, therefore, only can predict the ac loss generated by the perpendicular magnetic field. In contrast, the model based on H-formulation can be performed on the actual 2D rectangular cross section HTS tapes to provide the total ac losses generated by magnetic fluxes penetrating from both the edges and surfaces of HTS tapes, although this model requires more computing time and memory. The 1D and 2D simulation models were validated by cross comparing the results from both models and by comparing sub-section and full cross section models. Subsequently, two models relate cable design and operational parameters to the surface and edge losses of a two-layer CORC cable by considering the (1) relative contributions of edge and surface losses to the overall ac losses; (2) effect of the current distribution between inner and outer HTS layers on ac losses; (3) impact of the tape alignment on ac losses in each HTS layer; (4) influence of the thickness of HTS layers on ac losses; (5) effect of size and number of inter-tape gaps on ac losses; and (6) contribution frequency on the ac losses. The research results given in this paper are therefore not only valuable to suggest strategies for reducing ac loss in multi-layer cables but also for developing more accurate and effective methods to calculate ac loss in CORC HTS cables. [ABSTRACT FROM AUTHOR]
- Published
- 2023
- Full Text
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11. Copper ion concentration detection based on quantum weak measurement of circular dichroism.
- Author
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Tang, Tingting, Huang, Hua, Li, Jun, He, Yu, Li, Jie, Liang, Xiao, and Li, Chaoyang
- Subjects
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COPPER ions , *CIRCULAR dichroism , *TECHNOLOGICAL innovations , *METAL detectors , *TERNARY forms - Abstract
In this paper, a high precision detection method of copper ion (C u 2 + ) concentration based on weak measurement is proposed. The ternary complex formed by C u 2 + with L-tryptophan and phenanthroline reagents has circular dichroism (CD) signal at 605 nm in visible light. The CD signal can be obtained using the intensity contrast as a pointer in the imaginary weak-value amplification scheme. The measured sensitivity and resolution are 0.3417 mrad l/mg and 0.058 mg/l, respectively, which is improved by an order of magnitude compared to the traditional CD measurement method. It is also more accurate and less costly than commonly used C u 2 + detection methods. The C u 2 + concentration detection based on the weak measurement of CD signal detection proposed in this paper not only brings technological breakthroughs in the field of heavy metal ion detection, but also is of great significance in promoting the cross-development of chemistry, biomedicine, and life sciences. [ABSTRACT FROM AUTHOR]
- Published
- 2024
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12. Metasurface-based wireless communication technology and its applications.
- Author
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Cheng, Xinyue, Li, Chenxia, Fang, Bo, Hong, Zhi, Jin, Yongxing, and Jing, Xufeng
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WIRELESS communications , *TELECOMMUNICATION , *WIRELESS power transmission , *COMMUNICATION of technical information , *LITERATURE reviews - Abstract
Metasurfaces, due to their outstanding ability to control electromagnetic waves, have great application prospects in the field of wireless communication. This paper provides a comprehensive review of research work based on metasurface in three aspects: wireless power transfer, wireless information transmission, and novel wireless transceiver architectures. In the domain of wireless power transfer, several focusing metasurfaces and systems with unique performance are presented along with a new formula for calculating wireless power transfer. Concerning wireless information transmission section, the direct digital information transmission based on metasurface and the information transmission based on space-time-coding digital metasurface are introduced. Lastly, a simplified wireless transceiver with metasurfaces was introduced. The paper concludes with a discussion on the future directions of metasurfaces in the wireless communication domain. [ABSTRACT FROM AUTHOR]
- Published
- 2024
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13. Multi-scale modeling of shock initiation of a pressed energetic material III: Effect of Arrhenius chemical kinetic rates on macro-scale shock sensitivity.
- Author
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Parepalli, P., Nguyen, Yen T., Sen, O., Hardin, D. B., Molek, C. D., Welle, E. J., and Udaykumar, H. S.
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MULTISCALE modeling , *CHEMICAL kinetics , *CHEMICAL models , *PREDICTION models - Abstract
Multi-scale predictive models for the shock sensitivity of energetic materials connect energy localization ("hotspots") in the microstructure to macro-scale detonation phenomena. Calculations of hotspot ignition and growth rely on models for chemical reaction rates expressed in Arrhenius forms; these chemical kinetic models, therefore, are foundational to the construction of physics-based, simulation-derived meso-informed closure (reactive burn) models. However, even for commonly used energetic materials (e.g., HMX in this paper) there are a wide variety of reaction rate models available. These available reaction rate models produce reaction time scales that vary by several orders of magnitude. From a multi-scale modeling standpoint, it is important to determine which model best represents the reactive response of the material. In this paper, we examine three global Arrhenius-form rate models that span the range of reaction time scales, namely, the Tarver 3-equation, the Henson 1-equation, and the Menikoff 1-equation models. They are employed in a meso-informed ignition and growth model which allows for connecting meso-scale hotspot dynamics to macro-scale shock-to-detonation transition. The ability of the three reaction models to reproduce experimentally observed sensitivity is assessed by comparing the predicted criticality envelope (Walker–Wasley curve) with experimental data for pressed HMX Class V microstructures. The results provide a guideline for model developers on the plausible range of time-to-ignition that are produced by physically correct Arrhenius rate models for HMX. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
14. A compensation method of carrier magnetic interference under pathological conditions for geomagnetic navigation.
- Author
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Ji, Caijuan, Song, Chengying, Li, Sheng, Gao, Yang, and Chen, Qingwei
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LEAST squares , *MEASUREMENT errors , *GEOMAGNETISM , *ELECTRONIC equipment , *MAGNETOMETERS , *NAVIGATION - Abstract
Geomagnetic navigation has become a hot spot in current research because of its characteristics of passiveness and good concealment. However, the magnetic interference from various ferromagnetic substances, electronic equipment, etc., of the carrier will be superimposed on the geomagnetic field, causing magnetometer measurement errors, thus affecting navigation accuracy. In practice, due to the limited maneuverability of the carrier, sufficient geomagnetic observation data cannot be obtained, resulting in the observation equation used for carrier magnetic interference compensation to be seriously pathological. To achieve the compensation of carrier magnetic interference, this paper proposes the total least squares method based on the ridge regression using the L curve to solve ridge parameters. This method can effectively suppress the measurement noise that exists on both sides of the observation equation, and is suitable for alleviating the pathological effects of carrier magnetic interference compensation. Experimental results show that the compensated magnetometer measurement error is reduced to 3% of the carrier magnetic interference by using the method proposed in this paper, which obtains more stable and accurate parameter estimates. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
15. Piezoelectric energy harvester with outstanding output performance at low frequency vibration based on concentrating force on the piezoelectric element by parallel springs.
- Author
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Hao, Yifan, Luo, Hongzhi, Lu, Xinyue, Huang, Jiawei, Chen, Hang, and Yang, Tongqing
- Subjects
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FREQUENCIES of oscillating systems , *PIEZOELECTRIC ceramics , *STAINLESS steel , *LEAD titanate , *LEAD zirconate titanate - Abstract
This paper proposes a piezoelectric energy harvester that concentrates force on the piezoelectric element by parallel springs. When vibrating, the force exerted by the mass is released at three equal points on the surface of the brass substrate through three parallel springs. This concentrated release of energy through the spring amplification effect facilitates large deformation of the piezoelectric ceramic sheet, resulting in a higher charge output. The results show that under the combined action of a 14 g annular hollow mass and a 0.3 mm wire diameter stainless steel spring, the energy harvester based on the lead zirconate titanate ceramic exhibited an outstanding output power of 1.0–32.1 mW at a low resonance frequency with acceleration amplitudes of 0.5–3 g (1 g = 9.8 m/s2). More importantly, to match the vibration frequency of the actual environment, this paper optimized the structure of the harvester and proposed that the harvester can be designed by selecting the weight of the mass block, the parameters and number of springs, and the shape of the brass substrate. The energy harvester designed in this study is expected to capture energy from low-frequency natural environments and exhibit outstanding output performance, which can provide guidelines for future efforts in this direction. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
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16. High-volume biological sample processing using microwaves.
- Author
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Wilson-Garner, S., Alzeer, S., Baillie, L., and Porch, A.
- Subjects
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SAMPLING (Process) , *BACTERIAL DNA , *MICROWAVES , *DNA probes , *CAVITY resonators - Abstract
This paper describes the design and optimization of a 10 ml cartridge for patient sample processing using a 3.5 GHz (empty resonant frequency) TM010 cylindrical microwave cavity. The cartridge has been designed to augment a novel approach for the rapid diagnosis of M. tuberculosis (the causative agent of Ttuberculosis), which uses the direct application of microwaves to a bacteria-containing sample to release pathogen-specific DNA. The target bacterial DNA is then captured and recovered using magnetic nanoparticles coated with pathogen-specific DNA probes. Excitation parameters were optimized using three surrogates for M. tuberculosis, namely, M. smegmatis, M. abscessus, and M. bovis suspended in water and simulated sputum. The paper also explores the mechanism of microwave-mediated DNA release from bacteria using scanning electron microscopy. Examination of bacteria exposed to microwaves at power levels known to mediate the release of DNA reveals no obvious signs of permanent cell disruption, suggesting that a more subtle interaction is taking place. Finally, the presence of microwave-liberated M. bovis DNA was able to be detected at a level of sensitivity comparable to that achieved using microscopy. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
17. Study of electric-field induced ionic migration on all-inorganic perovskite CsPbBr3 single crystal nuclear radiation detector.
- Author
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Zhang, Mingzhi, Xia, Guotu, Huang, Chentao, Liu, Juan, Deng, Wenjuan, Tian, Fang, Zou, Jijun, and Tang, Bin
- Subjects
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NUCLEAR counters , *SINGLE crystals , *PEROVSKITE , *HYSTERESIS , *ACTIVATION energy , *ELECTRIC fields , *PHOTOELECTRICITY - Abstract
As one of the promising room temperature nuclear radiation detection materials, the all-inorganic perovskite CsPbBr3 single crystal has been receiving much attention in recent years. Even though the performance of the CsPbBr3 detector is improving continuously, the disadvantages of detection instability have not been solved fundamentally, and this instability is mainly caused by ionic migration in the CsPbBr3 single crystal itself. In this paper, a reasonable ionic migration model is proposed based on an in-depth study of the current hysteresis phenomenon and ionic migration mechanism in the Ti/CsPbBr3/Ti detector. The model shows that the ions migrate to the anode or cathode under an external electric field, and the accumulated ions subsequently form an inverted internal electric field inside the crystal and carrier transport barriers at the metal–semiconductor interface simultaneously. The photoelectric characteristic and ionic migration activation energy (E a i o n) fitting results also prove the rationality of the ionic migration model. Furthermore, the ionic migration model can also be used to explain the left-shift of the energy response peak and the decrease in the normalized charge collection efficiency in the Ti/CsPbBr3/Ti detector. This paper systematically investigates the intrinsic origin of migrated ions and the influence of ionic migration on detection stability, which will provide a potential solution to improve detection stability by suppressing ionic migration in the near future. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
18. X-ray texture analysis of paper coating pigments and the correlation with chemical composition analysis.
- Author
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Roine, J., Tenho, M., Murtomaa, M., Lehto, V.-P., and Kansanaho, R.
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SURFACES (Technology) , *PRINTING properties of paper , *PRINTING equipment , *X-ray spectroscopy , *SURFACE coatings - Abstract
The present research experiments the applicability of x-ray texture analysis in investigating the properties of paper coatings. The preferred orientations of kaolin, talc, ground calcium carbonate, and precipitated calcium carbonate particles used in four different paper coatings were determined qualitatively based on the measured crystal orientation data. The extent of the orientation, namely, the degree of the texture of each pigment, was characterized quantitatively using a single parameter. As a result, the effect of paper calendering is clearly seen as an increase on the degree of texture of the coating pigments. The effect of calendering on the preferred orientation of kaolin was also evident in an independent energy dispersive spectrometer analysis on micrometer scale and an electron spectroscopy for chemical analysis on nanometer scale. Thus, the present work proves x-ray texture analysis to be a potential research tool for characterizing the properties of paper coating layers. [ABSTRACT FROM AUTHOR]
- Published
- 2007
- Full Text
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19. Thin film versus paper-like reduced graphene oxide: Comparative study of structural, electrical, and thermoelectrical properties.
- Author
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Okhay, Olena, Gonçalves, Gil, Tkach, Alexander, Dias, Catarina, Ventura, Joao, da Silva, Manuel Fernando Ribeiro, Valente Gonçalves, Luís Miguel, and Titus, Elby
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GRAPHENE oxide , *THIN films , *CHEMICAL reduction , *HYDRAZINE , *SEMICONDUCTORS - Abstract
We report fabrication of reduced graphene oxide (rGO) films using chemical reduction by hydrazine hydrate and rGO paper-like samples using low temperature treatment reduction. Structural analysis confirms the formation of the rGO structure for both samples. Current-voltage (I-V) measurements of the rGO film reveal semiconductor behavior with the maximum current value of ~3×10-4A. The current for the rGO paper sample is found to be, at least, one order of magnitude higher. Moreover, bipolar resistance switching, corresponding to memristive behavior of type II, is observed in the I-V data of the rGO paper. Although precise values of the rGO film conductivity and the Seebeck coefficient could not be measured, rGO paper shows an electrical conductivity of 6.7×102S/m and Seebeck coefficient of -6μV/°C. Thus, we demonstrate a simplified way for the fabrication of rGO paper that possesses better and easier measurable macroscopic electrical properties than that of rGO thin film. [ABSTRACT FROM AUTHOR]
- Published
- 2016
- Full Text
- View/download PDF
20. A study on Arctic sea ice dynamics using the continuous spin Ising model.
- Author
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Wang, Ellen
- Subjects
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ISING model , *SEA ice , *STATISTICAL matching , *ENVIRONMENTAL sciences , *LATTICE dynamics , *STATISTICAL physics , *PERCENTILES - Abstract
The Ising model, initially proposed about 100 years ago to explain ferromagnetism and phase transitions, has become a central pillar of statistical physics and a powerful tool for diverse applications in other fields including environmental studies. In this paper, we introduce continuous spin values between −1 and +1 to a two-dimensional Ising model and utilize the generalized Ising lattice to simulate the dynamics of sea ice/water transition for a large area of 1500 km by 1500 km in the Arctic region. The simulation process follows the Metropolis-Hastings algorithm and incorporates an innovative factor to account for the inertia of spin value changes. Using the sea ice concentration data collected by the National Snow and Ice Data Center, our results exhibit striking similarity between the simulated and the observed ice melting and freezing dynamics, and two numerical measures from the simulation—the ice coverage percentage and the ice extent—match closely with the data statistics. Moreover, the model's best-fit parameters demonstrate the substantial impact of the external forces, which can be further enriched and linked to the environmental factors in other climate change research. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
21. Frequency mismatch analysis of hemispherical shell resonators with both radius and thickness imperfections.
- Author
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Deng, Kaixin, Zeng, Libin, Pan, Yao, Jia, Yonglei, Luo, Yiming, Tao, Yunfeng, and Yuan, Jie
- Subjects
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IMPERFECTION , *RESONATORS , *GYROSCOPES , *POSSIBILITY - Abstract
The hemispherical shell resonator (HSR) is the core element of the hemispherical resonator gyroscope (HRG), and its frequency mismatch is a key property influencing gyroscope accuracy. Investigating the mechanism of frequency mismatch is vital for improving the quality of HSRs and performance of HRGs. Midsurface radius imperfections and thickness imperfections are two principal causes of frequency mismatch, but their combined effects have rarely been discussed. This paper develops a model to comprehensively analyze the frequency mismatch of HSRs with both radius and thickness imperfections. The model derives a quantitative relation between the frequency mismatch and the two imperfections, and provides principles for evaluating dominant imperfections. To validate the model, we conduct experiments on a batch of 12 HSRs with random geometric imperfections. We apply the model in calculating the theoretical frequency mismatches of these HSRs, and the results agree well with the experimental data. The experiment also confirms that for macro-HSRs, thickness imperfections have a larger impact than radius imperfections, and the frequency mismatch is approximately linear to the fourth thickness harmonic. Our research can be a useful reference for the design and fabrication of HSRs and may open new possibilities for high-precision manufacture of HRGs. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
22. Near-infrared imaging of heat transfer behavior between gadolinium and fluid during magnetization/demagnetization process of magnetocaloric effect.
- Author
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Nguyen, The-Anh, Kakuta, Naoto, Uchida, Ken-ichi, and Nagano, Hosei
- Subjects
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MAGNETOCALORIC effects , *DEMAGNETIZATION , *MAGNETIC cooling , *THERMAL boundary layer , *MAGNETIZATION , *PHOTOTHERMAL effect , *MAGNETIC particle imaging - Abstract
This paper reports on the application of a near-infrared (NIR) imaging system for visualizing heat transfer dynamics from a bulk gadolinium (Gd) sample to the surrounding water during the magnetization/demagnetization process of the magnetocaloric effect (MCE). The suggested approach relied on the spectral variation in water absorption band at 1150 nm wavelength within the NIR spectrum. An experimental setup integrated a telecentric uniform-illumination system, a halogen lamp, and an NIR camera to enable real-time monitoring of a single magnetization and demagnetization cycle induced by an external magnetic field, which was generated by a permanent-magnet-based magnetic circuit. Two-dimensional absorbance images captured during this cycle clearly depicted the thermal energy generated by the MCE in water. Furthermore, an analysis of the thermal boundary layer and the quantification of heat transfer from Gd to water provided insights into the dynamics over time. These results indicated the potential of our NIR imaging techniques in optimizing thermal–fluid interactions within MCE systems, thereby improving the design and efficiency of magnetic refrigeration systems. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
23. Enhancing ferroelectric characterization at nanoscale: A comprehensive approach for data processing in spectroscopic piezoresponse force microscopy.
- Author
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Valloire, H., Quéméré, P., Vaxelaire, N., Kuentz, H., Le Rhun, G., and Borowik, Ł.
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PIEZORESPONSE force microscopy , *NANOMECHANICS , *ELECTRONIC data processing , *FERROELECTRIC thin films , *POTASSIUM niobate , *MACHINE learning , *HYSTERESIS loop - Abstract
Switching Spectroscopy Piezoresponse Force Microscopy (SSPFM) stands out as a powerful method for probing ferroelectric properties within materials subjected to incremental polarization induced by an external electric field. However, the dense data processing linked to this technique is a critical factor influencing the quality of obtained results. Furthermore, meticulous exploration of various artifacts, such as electrostatics, which may considerably influence the signal, is a key factor in obtaining quantitative results. In this paper, we present a global methodology for SSPFM data processing, accessible in open-source with a user-friendly Python application called PySSPFM. A ferroelectric thin film sample of potassium sodium niobate has been probed to illustrate the different aspects of our methodology. Our approach enables the reconstruction of hysteresis nano-loops by determining the PR as a function of applied electric field. These hysteresis loops are then fitted to extract characteristic parameters that serve as measures of the ferroelectric properties of the sample. Various artifact decorrelation methods are employed to enhance measurement accuracy, and additional material properties can be assessed. Performing this procedure on a grid of points across the surface of the sample enables the creation of spatial maps. Furthermore, different techniques have been proposed to facilitate post-treatment analysis, incorporating algorithms for machine learning (K-means), phase separation, and mapping cross correlation, among others. Additionally, PySSPFM enables a more in-depth investigation of the material by studying the nanomechanical properties during poling, through the measurement of the resonance properties of the cantilever–tip–sample surface system. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
24. Laterally coupled photonic crystal surface emitting laser arrays.
- Author
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Gautam, C., Pan, M., Chen, Y., Rotter, T. J., Balakrishnan, G., and Zhou, W.
- Subjects
- *
SURFACE emitting lasers , *PHOTONIC crystals , *CRYSTAL surfaces , *QUANTUM well devices , *SOLID-state lasers - Abstract
We propose and investigate a novel coherent laser array design based on laterally coupled photonic crystal surface-emitting lasers (PCSELs). As a new type of semiconductor laser technology, PCSELs have field confinement in a planar cavity and laser beam emission in the surface normal direction. By engineering lateral couplings between PCSELs with heterostructure photonic crystal designs, we can achieve coherent operations from an array of PCSELs. In this paper, we demonstrate coherent operation from a passively coupled PCSEL array design. We fabricated PCSEL array devices on a GaAs-based quantum well heterostructure at a target wavelength of 1040 nm. Experimental results show that the 2-by-2 PCSEL arrays have spectral linewidth of 0.14–0.22 nm. Beam combining performance was characterized by self-interference experiments. Similar coherency between the PCSEL array and single PCSEL device was observed. Our compact PCSEL array designs by passive lateral coupling have potential applications in fields of on-chip photonic computing, quantum, and information processing. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
25. 230-fold Enhancement of second-harmonic generation by coupled double resonances in a dolmen-type gold metasurface.
- Author
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Sun, Xiaoteng, Gui, Lili, Xie, Hailun, Liu, Yiwen, and Xu, Kun
- Subjects
- *
OPTICAL computing , *SECOND harmonic generation , *FANO resonance , *RESONANCE , *SERS spectroscopy , *NONLINEAR optics , *STOCHASTIC resonance - Abstract
Optical metasurfaces, artificial planar nanostructures composed of subwavelength meta-atoms, have attracted significant attention due to their ability to tailor optical nanoscale properties, making them a versatile platform for shaping light in both linear and nonlinear regimes. This paper reports on the realization of second harmonic generation (SHG) enhancement based on a dolmen-type gold metasurface containing two resonances. Nonlinear scattering theory is employed to numerically investigate the SHG enhancement phenomenon in the resonant metasurface. The periodic dolmen-type gold metasurface introduces a diffraction coupling effect between Fano resonance and surface lattice resonance (SLR), providing strong local-field enhancement and significantly enhancing the nonlinear effect. We analyze the influence of the coupling between Fano resonance and SLR on the SHG intensity and achieve a 230-fold enhancement in SHG intensity compared to the single resonance case by adjusting the periodicity of the metasurface. The SHG-enhanced gold metasurface may find applications in sensing, imaging, optical computing, and integrated nonlinear optics. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
26. Effect of copper in the stabilization of Al/CuO energetic semiconductor bridge.
- Author
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Li, Chen-Ming, Wang, Kai-Bing, Ji, Xiao-Gang, Dong, Xiao-Fen, and Wang, Duan
- Subjects
- *
THERMODYNAMICS , *IGNITION temperature , *COPPER oxide , *COPPER , *SEMICONDUCTORS , *DIFFERENTIAL scanning calorimetry , *PLASMA temperature - Abstract
The long-term storage performance of energetic multilayer nanofilms is of great significance for their applications. In this paper, it is proposed to add a 10 nm Cu barrier layer between Al/CuO composite films to increase their storage stability. The Al/CuO composite film and Al/Cu/CuO composite film were aged for 14 days in an environment with a relative humidity of 40% and a temperature of 71 °C. Scanning electron microscopy and differential scanning calorimetry were used to analyze the microstructure and thermodynamic properties of the energetic films before and after aging, and the electrical detonation performance and ignition ability of energy-containing semiconductor bridges were studied. The results indicate that after aging for 14 days in an environment with a relative humidity of 40% and a temperature of 71 °C, the Al layer of the Al/CuO composite film becomes thinner, the Al2O3 interface layer increases, and the heat release decreases. The interlayer microstructure of the Al/Cu/CuO energetic multilayer nanofilms did not change significantly, and the addition of a 10 nm Cu layer formed a low-temperature Al–Cu alloy, reducing the reaction initiation temperature from 626 to 570 °C. The critical ignition time and critical ignition energy of the Al/CuO-energetic semiconductor bridge (ESCB) increased, the flame duration shortened from 440 to 300 μs, the flame size decreased by 50%, the plasma temperature decreased, and aging had no significant effect on the electrical explosion performance of Al/Cu/CuO-ESCB. After aging for 14 days in an environment with a relative humidity of 40% and a temperature of 71 °C, the maximum ignition gap of B/KNO3 for Al/CuO-ESCB decreased from 1.4 to 1.2 mm, while the maximum ignition gap for Al/Cu/CuO-ESCB remained at 1.6 mm, which significantly improved the ignition performance and long storage performance of the energetic semiconductor bridge. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
27. Homogenized color-gradient lattice Boltzmann model for immiscible two-phase flow in multiscale porous media.
- Author
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Liu, Yang, Feng, Jingsen, Min, Jingchun, and Zhang, Xuan
- Subjects
- *
POROUS materials , *STOKES flow , *DRAG force , *SURFACE forces , *SEEPAGE , *TWO-phase flow , *LATTICE Boltzmann methods , *COMPOSITE structures - Abstract
In this paper, a homogenized multiphase lattice Boltzmann (LB) model is established for parallelly simulating immiscible two-phase flow in both solid-free regions (pore scale) and porous areas (continuum scale). It combines the color-gradient multiphase model with the Darcy–Brinkman–Stokes method by adding a term that includes surface force and drag force of porous matrix to multiple-relaxation-time LB equation in moment space. Moreover, an improved algorithm is proposed to characterize and implement the apparent wettability in the locally homogenized porosity field. Validations and test cases are given to demonstrate the accuracy and robustness of this new model, as well as its applicability for trans-scale fluid simulation of transport and sorption behavior from porous (Darcy flow) area to free (Stokes flow) area. For practicality, the two-phase seepage flow in a composite rock structure with multiscale pores is simulated by this new model, and the effects of viscosity ratio and wettability on the displacement process are discussed. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
28. Dielectric, elastic, and piezoelectric matrices of [001]-textured Mn-PMN-PZT ceramics.
- Author
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Tang, Mingyang, Liu, Xin, Wang, Yike, Ren, Xiaodan, Yang, Zheng, Xu, Zhuo, Geng, Liwei D., and Yan, Yongke
- Subjects
- *
PHASE transitions , *TRANSITION temperature , *DIELECTRICS , *PERMITTIVITY , *PIEZOELECTRIC ceramics , *CERAMICS , *HIGH temperatures - Abstract
[001]-textured 0.4P(Mg1/3Nb2/3)O3-0.25PbZrO3-0.35PbTiO3-0.5%MnO2 (Mn-PMN-PZT) ceramics were fabricated by templated grain growth using 2 vol. % BaTiO3 in this paper. Full matrices of dielectric (ɛij), elastic (sij, cij), and piezoelectric (dij) parameters were obtained by the resonance–antiresonance method. The dielectric constant ɛ33T of textured ceramics reaches 2600, which is four times that of random ceramics. Textured Mn-PMN-PZT ceramics exhibit high d33 = 984 pC/N and high k33 = 0.89, which is much larger than d33 = 223 pC/N and k33 = 0.70 of random ceramics. However, ɛ11T of ceramics decreases by about 30% after texturing, and the corresponding shear coupling coefficient k15 also decreases from 0.66 to 0.44, which may be due to the reduction in the angle between spontaneous polarization and transverse direction. Furthermore, the temperature stability of the textured ceramics was evaluated as well. The phase transition temperature TR−T was determined by the impedance method to be 120 °C. The textured Mn-PMN-PZT ceramic shows high temperature stability, which is better than PMN-PT. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
29. Inerter-controlled topological interface states in locally resonant lattices with beyond-nearest neighbor coupling.
- Author
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Cajić, Milan, Karličić, Danilo, and Adhikari, Sondipon
- Subjects
- *
RESONANT states , *NOBLE gases , *ENERGY harvesting , *SYMMETRY breaking , *UNIT cell , *QUANTUM spin Hall effect - Abstract
This paper explores the emergence of topological interface states in one-dimensional locally resonant lattices incorporating inerters in both nearest neighbor (NN) and beyond-nearest neighbor (BNN) coupling. The investigation focuses on the unique wave propagation characteristics of these lattices, particularly the presence and behavior of interface states. The non-trivial topological behavior due to broken inversion symmetry within the unit cell of the locally resonant lattice is comprehensively investigated in the presence of inerters in NN and BNN coupling. The emerging interface states in the supercell analysis exhibit specific spatial and frequency localization properties due to inerter-based BNN interactions. Additionally, the study demonstrates the ability of inerter elements with weak inertance to control the frequency of interface states while maintaining the fundamental topological properties of the lattice. The identified topological interface states in lattices with BNN coupling present an opportunity for designing diverse devices, such as waveguides, filters, sensors, and energy harvesting systems. Overall, this research enhances our comprehension of topological phenomena in inerter-based locally resonant lattices with BNN interactions and introduces possibilities for creating robust and versatile devices based on topologically protected edge/interface states. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
30. Impact of the recessed gate depth on the GaN metal-oxide-semiconductor high electron mobility transistor performances: New insights on mobility extraction.
- Author
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Piotrowicz, C., Mohamad, B., Malbert, N., Bécu, S., Ruel, S., and Le Royer, C.
- Subjects
- *
METAL oxide semiconductor capacitors , *MODULATION-doped field-effect transistors , *METAL oxide semiconductor field-effect transistors , *GALLIUM nitride , *ELECTRON mobility , *COMPUTER-aided design , *PLASMA etching , *STRAY currents - Abstract
This paper provides a comprehensive study of the impact of the gate recess depth (RD) on the GaN-on-Si MOS-HEMTs DC performances. IDS = f(VGS) and IDS = f(VDS) measurements are conducted at 25 and 150 °C, respectively, in forward and blocking modes. The gate recessed depth (50, 150, and 350 nm) is modulated by adjusting the plasma etching time, which is a critical step for improving the dielectric/GaN interface quality and the gate channel electron mobility. Three distinct regions can be defined separately: the bottom, the sidewall, and the corner region being the junction between the two previous regions. To assess the impact of gate recessed depth (RD) on the several mobilities around the gate cavity first, we applied our previous methodology allowing us to extract the bottom (μbot) and the entire sidewall region mobility (μT), without distinction from the corner. The mobility of the transverse region was found surprisingly to increase with deeper RD. To gain insight into the impact of the RD on this transverse section, a new extraction methodology is proposed to extract separately the gate corner (μcorner) and sidewall (μSW) mobility. These extractions show that the corner mobility is found to be reduced compared to the sidewall one (μcorner < μSW) evidencing the different weighting contributions over the transverse mobility. Moreover, these mobilities are found to be more degraded compared to the bottom one, highlighting the different contributions on the on-state resistance (RON). Indeed, the on-state resistance is lowered with the shallower RD due to the reduced sidewall resistance contribution (lower sidewall length) and despite the incremental contribution of the bottom resistance (larger effective gate length). However, the shallower RD shows an increase in the drain–source leakage current in reason of a lower gate electrostatic control. Technology Computer Aided Design (TCAD) simulations of the three RD morphologies are carried out to validate the experimental trends and the proposed methodology. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
31. A novel lidar signal denoising method based on variational mode decomposition optimized using whale algorithm.
- Author
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Zhao, Lin and Mao, Jiandong
- Subjects
- *
METAHEURISTIC algorithms , *SIGNAL denoising , *HOUGH transforms , *LIDAR , *HILBERT-Huang transform , *SINGULAR value decomposition , *NOISE control - Abstract
Original lidar return signals are covered by high levels of noise that seriously affect the accuracy of subsequent data processing and inversion. Therefore, it is important to separate the effective signal from the returned signal with noise interference. In this paper, an efficient denoising method based on the variational mode decomposition (VMD) algorithm optimized using the global search strategy-based whale algorithm and the total variational stationary wavelet transform (GSWOA-VMD-SWTTV) is proposed, and this method is applied to denoising of lidar return signals. First, the global search strategy-based whale optimization algorithm (GSWOA) is used to acquire the optimal parameters of the VMD algorithm adaptively, and the lidar return signal is then decomposed by global search strategy-based whale optimization algorithm (GSWOA)-VMD. The effective modal components are then determined using the cross-correlation coefficient method from the decomposed modal components, and total variation stationary wavelet denoising is performed on each effective mode. Finally, the effective modes are reconstructed to obtain a clean lidar return signal. Moreover, to provide further verification of the effectiveness of the proposed method, it is compared with the ensemble empirical mode decomposition (EEMD) method, the complete EEMD with adaptive noise (CEEMDAN) method, the singular value decomposition (SVD) method, and the wavelet threshold method under sunny, cloudy, and dusty weather conditions. The experimental results demonstrate the superior noise reduction performance of the proposed algorithm, which can filter out strong noise from the signal while retaining the complete signal details without distortion; additionally, the proposed method has the highest signal-to-noise ratio and lowest mean square error. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
32. 2D analysis of sputtered species transport in high-power impulse magnetron sputtering (HiPIMS) discharge.
- Author
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Kapran, Anna, Ballage, Charles, Hubička, Zdeněk, and Minea, Tiberiu
- Subjects
- *
QUARTZ crystal microbalances , *MAGNETRON sputtering , *MAGNETIC separators , *THIN films , *SPECIES distribution , *TRANSPORT theory , *SPECIES - Abstract
Among the numerous advantages of the high-power impulse magnetron sputtering (HiPIMS) technique, the most important is the enhanced ionization degree of sputtered species contributing to the film growth. Consequently, the quality of deposited thin films is highly improved. Still, the optimization process is challenging due to the complexity associated with the intricate transport of the sputtered species, ionized or neutrals. The scarce knowledge available on the spatial distribution of these species when operating a HiPIMS discharge makes the quantitative prediction of any deposition feature particularly difficult. In this paper, we discuss the influence of experimentally controllable quantities, such as gas pressure and target current density, on the transport of sputtered titanium in non-reactive (argon) HiPIMS, namely, on the behavior of metal atoms and metal ion fluxes intercepting the substrate. Systematic quantitative measurements were performed in a diameter normal plane on a circular planar target. Hence, the 2D spatial distribution of the ionized flux fraction (IFF) and the total flux of titanium sputtered particles (deposition rate) are evaluated by biasing a quartz crystal microbalance equipped with an electron magnetic filter. The wide range of parameters we examined allows us to predict and optimize the flux of sputtered species based on complete mapping of the IFF of sputtered particles. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
33. Computational analysis of the anode-directed streamers propagation in atmospheric pressure C4F7N/N2 mixtures.
- Author
-
Levko, Dmitry, Thiruppathiraj, Sudharshanaraj, and Raja, Laxminarayan L.
- Subjects
- *
ELECTRIC breakdown , *BREAKDOWN voltage , *ATMOSPHERIC pressure , *TWO-dimensional models , *MIXTURES , *ELECTRONEGATIVITY - Abstract
In recent years, interest in synthetic C4F7N as a gas insulator has been growing due to its unique insulation properties and low global warming potential. In spite of this, very few studies are devoted to the analysis of the electric breakdown of C4F7N and its mixtures with other dilutants such as CO2 and N2. In the present paper, we use a two-dimensional fluid model to analyze the electrical breakdown of the atmospheric pressure C4F7N/N2 mixture. We establish the influence of the C4F7N fraction in the mixture and the cathode voltage rise rate on the breakdown voltage. We find that the ratio between the electron attachment frequency and the voltage rise rate defines the streamer parameters. Namely, if the time scale of electron attachment to C4F7N is much faster than the voltage rise rate, the plasma electronegativity of the streamer body and of its head is extremely high, and it is difficult to define exactly the streamer head location. In the opposite case of the fast rise rates, the conventional streamers with sharp heads were obtained. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
34. Theoretical modeling of defect diffusion in wide bandgap semiconductors.
- Author
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Knausgård Hommedal, Ylva, Etzelmüller Bathen, Marianne, Mari Reinertsen, Vilde, Magnus Johansen, Klaus, Vines, Lasse, and Kalmann Frodason, Ymir
- Subjects
- *
WIDE gap semiconductors , *SEMICONDUCTOR defects , *CRYSTALS , *KIRKENDALL effect , *DENSITY functional theory , *CRYSTAL defects , *SECONDARY ion mass spectrometry - Abstract
Since the 1940s, it has been known that diffusion in crystalline solids occurs due to lattice defects. The diffusion of defects can have a great impact on the processing and heat treatment of materials as the microstructural changes caused by diffusion can influence the material qualities and properties. It is, therefore, vital to be able to control the diffusion. This implies that we need a deep understanding of the interactions between impurities, matrix atoms, and intrinsic defects. The role of density functional theory (DFT) calculations in solid-state diffusion studies has become considerable. The main parameters to obtain in defect diffusion studies with DFT are formation energies, binding energies, and migration barriers. In particular, the utilization of the nudged elastic band and the dimer methods has improved the accuracy of these parameters. In systematic diffusion studies, the combination of experimentally obtained results and theoretical predictions can reveal information about the atomic diffusion processes. The combination of the theoretical predictions and the experimental results gives a unique opportunity to compare parameters found from the different methods and gain knowledge about atomic migration. In this Perspective paper, we present case studies on defect diffusion in wide bandgap semiconductors. The case studies cover examples from the three diffusion models: free diffusion, trap-limited diffusion, and reaction diffusion. We focus on the role of DFT in these studies combined with results obtained with the experimental techniques secondary ion mass spectrometry and deep-level transient spectroscopy combined with diffusion simulations. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
35. An exploration of anomalous electrical noise in shocked cyclotrimethylenetrinitramine (RDX)-based explosives.
- Author
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Burns, M. J. and Chidester, B. A.
- Subjects
- *
ELECTRIC noise , *CYCLONITE , *ELECTROMAGNETIC noise , *EXPLOSIVES , *PHASE diagrams , *BLAST effect - Abstract
Gas gun shock experiments on cyclotrimethylenetrinitramine (RDX)-based explosive compositions that employ embedded gauge particle velocity tracers have noted a significant amount of electrical noise when compared to other explosive formulations. This paper reexamines previously published embedded gauge data on Cyclotols (60–80 wt. % RDX) to quantify the electromagnetic behavior of these materials. The primary observation is a fourfold increase in the electrical noise when Cyclotols are shocked above 4.22 ± 0.08 GPa. Electromagnetic gauge noise is also observed within particle velocity traces in reactive growth and off-Hugoniot shocks, although at higher pressures than the direct shock case, suggesting a temperature- or kinetically dependent transition. In all cases, the electrical noise disappears upon detonation. By comparing with the static high-pressure phase diagram of RDX, we interpret this change in electromagnetic behavior to be a change in the RDX crystal structure to a piezoelectric phase, although it is uncertain whether the γ or ε phase is responsible for the observed behavior. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
36. Unraveling the impact of initial choices and in-loop interventions on learning dynamics in autonomous scanning probe microscopy.
- Author
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Slautin, Boris N., Liu, Yongtao, Funakubo, Hiroshi, and Kalinin, Sergei V.
- Subjects
- *
SCANNING probe microscopy , *PIEZORESPONSE force microscopy , *DEEP learning , *SELF-tuning controllers , *KELVIN probe force microscopy , *THIN films , *WORKFLOW - Abstract
The current focus in Autonomous Experimentation (AE) is on developing robust workflows to conduct the AE effectively. This entails the need for well-defined approaches to guide the AE process, including strategies for hyperparameter tuning and high-level human interventions within the workflow loop. This paper presents a comprehensive analysis of the influence of initial experimental conditions and in-loop interventions on the learning dynamics of Deep Kernel Learning (DKL) within the realm of AE in scanning probe microscopy. We explore the concept of the "seed effect," where the initial experiment setup has a substantial impact on the subsequent learning trajectory. Additionally, we introduce an approach of the seed point interventions in AE allowing the operator to influence the exploration process. Using a dataset from Piezoresponse Force Microscopy on PbTiO3 thin films, we illustrate the impact of the "seed effect" and in-loop seed interventions on the effectiveness of DKL in predicting material properties. The study highlights the importance of initial choices and adaptive interventions in optimizing learning rates and enhancing the efficiency of automated material characterization. This work offers valuable insights into designing more robust and effective AE workflows in microscopy with potential applications across various characterization techniques. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
37. AlGaN/GaN bilateral IMPATT device by two-dimensional electron gas for terahertz application.
- Author
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Dai, Yang, Li, Yukun, Gao, Leiyu, Zuo, Jing, Zhang, Biying, Chen, Cheng, Wang, Zhongxu, and Zhao, Wu
- Subjects
- *
TWO-dimensional electron gas , *MODULATION-doped field-effect transistors , *GALLIUM nitride , *OHMIC contacts , *ELECTRON gas , *MANUFACTURING processes , *TERAHERTZ spectroscopy - Abstract
A novel bilateral impact-ionization-avalanche-transit-time (BIMPATT) diode based on AlGaN/GaN two-dimensional electron gas is proposed in this article. The BIMPATT is compatible with the available GaN high electron mobility transistor (HEMT) manufacturing process and has a shorter actual electron transit distance than existing HEMT-like IMPATT (HIMPATT) diodes. Compared with the same-sized HIMPATT, the optimum frequency of BIMPATT rises from 320 to 420 GHz and possesses a far wider operating frequency band, especially in the near 0.9 THz range. The maximum DC-RF conversion efficiency rises from 12.9% to 17.6%. The maximum RF power of BIMPATT is 3.18 W/mm, which is similar to 3.12 W/mm of the HIMPATT. Furthermore, our simulation demonstrated that the characteristics of BIMPATT are significantly affected by the length of anode and the thickness of the AlGaN barrier layer. The effects of ohmic contact resistance and background impurities on BIMPATT are also taken into account. This paper provides a reference for the design and characteristics enhancement of the lateral IMPATT devices. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
38. Magnetic properties of Fe56Pd44−xGdx thin films.
- Author
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Sahari, Mohamed Abdennour, Olivetti, Elena Sonia, Magni, Alessandro, Fiore, Gianluca, Boudissa, Mokhtar, Tiberto, Paola, Bahamida, Saida, and Coïsson, Marco
- Subjects
- *
MAGNETIC properties , *THIN films , *EXCHANGE interactions (Magnetism) , *MAGNETIC force microscopy , *MAGNETIC domain , *GADOLINIUM - Abstract
In this paper, we have studied the effect on the structure and magnetic properties of partial Pd substitution by Gd in Fe–Pd thin films of nominal composition Fe56Pd44−xGdx (x = 1, 3, 5, and 7), deposited onto Si(100) and Si(100)/SiO2 substrates by thermal evaporation. Several techniques contribute to the characterization of their microstructure and magnetic properties, such as x-ray diffraction (XRD), scanning electron microscopy, alternating gradient field magnetometry, and magnetic force microscopy (MFM). X-ray diffraction shows that the as-deposited films are either amorphous or contain a disordered FePd phase, depending on the film thickness. The transformation of disordered fcc-FePd into ordered fct-FePd has been induced by a heat treatment at 530 °C for 4 h. The addition of gadolinium leads to a reduction in the coercivity as a consequence of the emergence of soft phases and of the progressive reduction of the fct-FePd phase, which is primarily responsible for the observed maze magnetic domains. The exchange coupling between the soft phase and the hard fct-FePd phase is demonstrated by first-order reversal curves (FORCs). [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
39. Plasma assisted remediation of SiC surfaces.
- Author
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Mathews Jr., M. A., Graves, A. R., Boris, D. R., Walton, S. G., and Stinespring, C. D.
- Subjects
- *
X-ray photoelectron spectroscopy , *ATOMIC force microscopy , *ATOMIC spectroscopy , *HYDROFLUORIC acid , *SURFACE defects - Abstract
This paper describes a three-step process to remediate surface and sub-surface defects on chemo-mechanically polished SiC surfaces. In this process, a CF4-based inductively coupled plasma with reactive ion etch was used to remove material to a depth, which is unaffected by surface and subsurface polishing damage. This produced a planarized but carbon-rich fluorinated surface. This surface was then exposed to a 2 min rapid thermal oxidation in air at 1000 °C to oxidize and volatilize the excess carbon and fluorinated species, respectively. The resulting surface oxide was then stripped using a dilute hydrofluoric acid in water solution. This process, referred to as plasma assisted remediation, reproducibly yielded planarized, stoichiometric surfaces with low levels of carbon and oxygen contamination suitable for subsequent device fabrication. In the supporting studies described here, 4H- and 6H-SiC(0001) surfaces were remediated and characterized by x-ray photoelectron spectroscopy and atomic force microscopy at each stage of the process. Experimental studies under ion-rich and radical-dominant conditions are also reported which provide greater insight into the underlying chemistry and physics of the process. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
40. Merging of TM-polarized bound states in the continuum in leaky-mode photonic lattices.
- Author
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Lee, Sun-Goo, Kim, Seong-Han, Suk Hong, Kee, and Lee, Wook-Jae
- Subjects
- *
BOUND states , *FINITE element method , *OPTICAL devices , *MOMENTUM space , *OPTICAL spectra , *BAND gaps - Abstract
Optical eigenstates with a high quality (Q) factor provide substantial advantages for a broad spectrum of optical devices, particularly those demanding strong light–matter interactions. Recently, it has been demonstrated that ultrahigh- Q resonances can be realized in planar photonic structures by merging multiple bound states in the continuum (BICs) in the momentum space. Photonic lattices with thin-film geometry are known to support abundant TE-polarized and TM-polarized BICs. While prior research has explored the merging of TE-polarized BICs, this paper presents analytical and numerical results concerning the merging of TM-polarized BICs in laterally periodic one-dimensional photonic lattices. As the thickness of photonic lattices increases, TM-polarized accidental BICs descend along the dispersion curves and eventually merge at the upper edge of the second stop band. Employing coupled-mode analysis, we calculate the analytical merging thickness at which multiple TM-polarized BICs come together at the second-order Γ point. We confirm the merging of TM-polarized BICs through finite-element method simulations. Our results can be beneficial for achieving ultrahigh- Q resonances through the merging of BICs. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
41. Measurement of coating–substrate interface stiffness using a constructed ultrasonic echo phase derivative spectrum.
- Author
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Qi, Tianzhi, Lin, Li, Ma, Zhiyuan, Yang, Jiwei, and Zhao, Yang
- Subjects
- *
ECHO , *ULTRASONICS , *ULTRASONIC welding , *CARBON steel , *REFLECTANCE - Abstract
Measurement of coating–substrate interface stiffness can indirectly characterize interface bonding quality. This paper proposes a noval quantitative inversion coating–substrate interface stiffness method based on the multi-resonance frequencies of a constructed ultrasonic echo phase derivative spectrum (UEPDS). The theoretical relationship between UEPDS resonance frequencies and interface stiffness is derived. The detection frequency and high-sensitivity interface stiffness range are optimized based on the sensitivity analyzed. Numerical simulation and experiment are implemented on a 0.48 mm aluminum layer/carbon steel substrate specimen to prove the validity of the proposed ultrasonic method. The simulation results show that the maximal relative error between the inversion and the preset interface stiffnesses is reduced from 23% to 8% compared with the traditional ultrasonic reflection coefficient amplitude spectrum-based (URCAS-based) method. The experiment results indicate that the UEPDS-based inversion interface stiffnesses have the same trend as the nominal contact pressures between the coating–substrate interface. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
42. A wideband high-gain dielectric resonator antenna based on mullite microwave dielectric ceramics.
- Author
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Du, Chao, Bao, Ziyan, Chen, Hetuo, Zhou, Guohong, Pang, Yongqiang, Liu, Haiwen, Jiang, Huangfu, Zhou, Tao, Xia, Song, and Zhou, Di
- Subjects
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DIELECTRIC resonator antennas , *MICROWAVE devices , *MULLITE , *MICROWAVES , *DIELECTRICS , *DIELECTRIC properties - Abstract
In this paper, the high-quality factor mullite microwave dielectric ceramic is employed to introduce in dielectric resonator antenna (DRA). The microwave dielectric properties of ɛr ∼ 5.8, Q × f ∼ 31 240 at 9.66 GHz, and loss tangent tanδ = 1/Q ∼ 2.7 × 10−4 can be obtained by the solid-state reaction method in mullite microwave dielectric ceramic sintered at 1700 °C. On this basis, the resonant modes of the proposed broadband high-gain rectangular DRA are analyzed by using a dielectric waveguide theoretical model and the antenna performance is evaluated by a commercial CST Microwave Studio 2021® software. It has been found that the proposed rectangular DRA can provide a broad bandwidth of 35.9%, a maximum gain of 10 dBi at 3.61 GHz, and a radiation efficiency of 90% in the range of 3.13–4.42 GHz. For demonstration, adequate consistency between the simulation results and the measurement results was achieved. The proposed DRA has great application potential and value in 5G communication scenarios requiring wideband and high-gain antenna. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
43. Analysis and modeling of the influence of gate leakage current on threshold voltage and subthreshold swing in p-GaN gate AlGaN/GaN high electron mobility transistors.
- Author
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Liu, Kai, Wang, Chong, Zhang, Kuo, Ma, Xiaohua, Bai, Junchun, Zheng, Xuefeng, Li, Ang, and Hao, Yue
- Subjects
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THRESHOLD voltage , *MODULATION-doped field-effect transistors , *STRAY currents , *GALLIUM nitride , *METALWORK , *FIELD-effect transistors , *SCHOTTKY barrier - Abstract
In this paper, the p-GaN gate AlGaN/GaN high electron mobility transistors (HEMTs) with varying combinations of gate metal work function and gate geometry are fabricated and investigate the influence of gate leakage current (IGS) on the threshold voltage (VTH) and subthreshold swing (SS). The unique dependence of VTH and SS on gate geometry for different metals is observed, which is different from traditional field-effect transistors. A novel hybrid physics model, consisting of the traditional capacitance divider model and hole injection model, is proposed to explain this phenomenon, and the results exhibit an excellent agreement with the experimental data. The holes traverse the gate/p-GaN Schottky barrier by thermal emission or tunneling and inject into the p-GaN layer, generating the IGS. Expanding upon the traditional capacitance divider model, a portion of the injected holes accumulate at the p-GaN/AlGaN interface and induce the corresponding electrons at the AlGaN/GaN heterojunction, which promotes channel conduction. Hence, the transfer curves display the correlation between IGS and VTH as well as SS. The results show that high IGS can alleviate the instability of VTH caused by the lithographic overlay error, and simultaneously optimize SS. This work offers a novel perspective for examining the turn-on mechanism of p-GaN HEMTs, thereby contributing to device design. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
44. Electromagnetic absorption properties of FexCoNi magnetic nano particles.
- Author
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Li, Hong, Li, Hongyang, Yang, Feng, Cai, Qing, Xu, Wenqi, Wang, Ran, and Liu, Ying
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- *
MAGNETIC permeability , *MAGNETIC properties , *PERMITTIVITY , *MAGNETIC particles , *MAGNETIC flux leakage , *DIELECTRIC loss - Abstract
The microstructure morphology, static magnetic properties, and electromagnetic absorption characteristics of nano FexCoNi alloy particles prepared by chemical liquid deposition with five different Fe content levels are investigated in this paper. The results show that spherical FexCoNi alloy particles with an average particle size of about 100–200 nm and a face-centered cubic crystal structure were obtained. All five samples exhibited soft magnetic behavior, with the saturation magnetization intensity showing an increasing-then-decreasing trend with increasing Fe content, peaking at 141.8 emu/g for Fe content x = 1.0. The dielectric constants (real and imaginary parts) of the prepared alloy particles exhibit significant differences with respect to the variation of Fe content, while the changes in the real and imaginary parts of the magnetic permeability show less pronounced effects with increasing Fe content. As the electromagnetic wave frequency increases, the real parts of the dielectric constants for all composites show minimal fluctuations, and the real parts of the magnetic permeability exhibit a decreasing trend. Moreover, the imaginary parts of the dielectric constants and magnetic permeability show an increasing followed by a decreasing trend as the frequency rises. The material with Fe content x = 1 demonstrated optimal dielectric loss performance and relatively excellent magnetic loss performance, with a sample thickness of 1.9 mm exhibiting the highest reflection loss (RLmax) of −24.2 dB and an effective absorption bandwidth of 4.48 GHz. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
45. Amplitude and phase modulation with electric quadrupole radiation.
- Author
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Zhang, Jiawei, Shi, Weijie, Liu, Andong, Tang, Lili, Zhang, Shuyan, and Dong, Zhenggao
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PHASE modulation , *QUADRUPOLES , *RADIATION , *REFRACTION (Optics) , *GEOMETRIC quantum phases - Abstract
Optical metasurfaces can be used to realize various peculiar optical effects, and their mechanisms of the controlling optical phase can be roughly categorized into three types: resonant phase, geometric phase, and propagation phase, also known as the dynamic phase. Multiple mechanisms can be employed to manipulate the phase and amplitude of one metasurface. Therefore, discovering more profound and diverse methods can provide additional degrees of application freedom. This paper proposes a control principle based on electric multipole expansion. We found that for a unit structure formed by dual-metal bars on a metasurface, the radiation of its dipole is equivalent to the interference results of the dual-metal bars. Moreover, the radiation of the quadrupole enables independent control for amplitude and phase. Therefore, we used quadrupole radiation to manipulate the phase and amplitude of the light and even investigated some simple applications, including the realization of focusing light and anomalous refraction. Such a new mechanism of controlling light, combined with other methods, can provide significant insights into achieving challenging goals, like steganography and multifunctional metasurfaces. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
46. A ternary complementary Gray code phase unwrapping method in fringe projection profilometry.
- Author
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Wei, Hao, Li, Hongru, Liu, Jiangtao, Deng, Guoliang, and Zhou, Shouhuan
- Subjects
- *
GRAY codes , *PHASE coding , *BINARY codes - Abstract
This paper proposes a phase unwrapping method based on ternary Gray code in fringe projection profilometry. This method does not require additional projection images or any prior knowledge. It accurately determines the segmentation thresholds of the ternary Gray code using only the average intensity and intensity modulation calculated from phase-shifting fringes, effectively reducing projection costs and achieving lower codeword errors. Additionally, a segment selection strategy suitable for the ternary Gray code is proposed. By employing the complementary method, three sets of candidate orders with certain codeword shifts can be generated. The wrapped phase is then divided into three segments: upper, middle, and lower segments, and correspondingly matched with the central regions of the three sets of candidate orders, thus enabling the solution of the absolute phase. Through the segment selection strategy, error-prone areas at the edges of orders are effectively avoided, further enhancing the accuracy of measurement results. Compared to the binary Gray code, the ternary complementary Gray code can encode up to 3 m − 1 orders when the number of Gray code patterns is m; when the required number of encoding orders is K, only ⌈ log 3 K ⌉ + 1 Gray code patterns are needed. Its additional value capacity precisely enables it to encode more orders, thereby increasing the frequency of phase-shifting fringes and further enhancing measurement efficiency. A series of experiments validates the feasibility, robustness, and superiority of this method. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
47. A multi-party verifiable quantum proxy signature scheme based on quantum teleportation.
- Author
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Wang, Chengxiang, Lu, Dianjun, Tian, Fuyao, and Yao, Weixin
- Subjects
- *
QUANTUM teleportation , *PROBLEM solving , *CRYPTOGRAPHY - Abstract
With the development of science and technology and the appearance of various special conditions that cause signers to be unable to sign, proxy signature is gradually becoming a hot spot in cryptography research. This paper combines proxy signature, quantum teleportation, and multi-party verification and proposes a multi-party verifiable quantum proxy signature scheme based on quantum teleportation. This scheme has the following characteristics: The authentication method based on the H a s h function can effectively solve the problem of identity identification among members; in order for the proxy signer to be able to verify the correctness of the proxy authorization, a form of proxy signature authorization that concatenates the identity information of the original signer is used. The security analysis shows that our scheme is unforgeable and undeniable and can resist intercept-resend attacks and cheating attacks. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
48. Structurally tunable acoustic transmission-coded metamaterials.
- Author
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Cui, Qinghao, Wang, Jilai, Tang, Xuefeng, Li, Quhao, Men, Junhui, and Wan, Yi
- Subjects
- *
SOUND waves , *METAMATERIALS , *FRESNEL lenses , *PLANE wavefronts , *SPACE frame structures , *TRANSMISSION of sound - Abstract
The introduction of metasurfaces has renewed Snell's law, and the metasurfaces can manipulate sound waves flexibly. In this paper, a coding metasurface with a simple and adjustable coding unit for sound wave transmission is proposed. By changing the orientation of a movable part in a fixed structure, conversion is achieved between two types of units with a phase difference of 180° and high transmittance (>75%). By combining the two types of units, the phases of sound waves can be regulated dynamically. Structural simulations are performed using finite-element software, and the beam splitting of the transmitted sound wave is verified by theoretical analysis and experiments under plane wave incidence in the frequency range of 4.7–5.7 kHz. In addition, the two types of units are used to design a coding Fresnel lens, and its simulated focusing performance is verified by experiments at 4.7–5.7 kHz. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
49. Investigation of the areas with high D07-band emission in multicrystalline silicon wafers using electron microscopy and hyperspectral photoluminescence imaging.
- Author
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Thøgersen, Annett, Jensen, Ingvild J. T., Mehl, Torbjørn, Burud, Ingunn, Olsen, Espen, Gudem Ringdalen, Inga, Zhu, Junjie, and Søndenå, Rune
- Subjects
- *
SILICON wafers , *SCANNING transmission electron microscopy , *SILICON solar cells , *FOCUSED ion beams , *PHOTOLUMINESCENCE , *PHOTOLUMINESCENCE measurement - Abstract
This paper explores the fundamental structural origins of the 0.7 eV band emission peak, known as D07. The increased attention on these d-band emission lines originates mainly from the correlation between crystal defect and the intensified recombination of less dominant charge carriers. This association holds substantial importance, impacting not just the electronics sector but also raising concerns about reduced efficiency in silicon solar cells. By employing hyperspectral photoluminescence imaging, we pinpointed regions manifesting high D07 peak emissions on a microscopic scale. Subsequently, we conducted a structural investigation utilizing scanning electron microscopy and electron backscatter diffraction. Following this, we used a focused ion beam to extract areas of interest, allowing for a detailed characterization of the sample using high-resolution scanning transmission electron microscopy at the atomic scale. This approach aids in identifying defects and determining grain boundary orientation. In areas of high D07 band emission, we found Σ 3 { 114 } { 101 } grain boundaries decorated with two-layer fault twin and/or an extrinsic two-layer stacking faults. In addition, density functional theory calculations suggest oxygen impurities as a possibility for substitutional segregation to these types of defects. It is therefore plausible that the D07 line might be attributed to stacking faults featuring oxygen agglomerates. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
50. Thermophysical characterization of artificially aged papers by means of the photothermal...
- Author
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Bertolotti, M. and Ligia, S.
- Subjects
- *
PAPER , *THERMOPHYSICAL properties - Abstract
Presents information on a study which determined the thermophysical properties of artificially aged paper samples by means of photothermal deflection technique. Theory; Experimental results and discussion; Conclusions.
- Published
- 1999
- Full Text
- View/download PDF
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