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A woman's crown made of fine gilt bronze with refined glass inlay work was excavated from a Sui-Tang tomb called Kunlun M2 in Xi'an, Shaanxi Province, China. Very few female crowns and crown ornaments have been excavated in China thus far, and there has been a lack of systematic research into the technologies used to manufacture them. Importantly, this paper uses the M2 crown to investigate its surface inlays and overall shape, then conducts a comparative analysis of women's crown ornaments of the same type, providing a reference for study of the crown. Non-invasive and micro-destructive analysis including optical microscopy (OM), optical coherence tomography (OCT), micro X-ray fluorescence imagery (XRF), and Raman spectroscopy were applied. These identified the crown's inlays as potash-lime glass, composed mainly of the raw materials: vein quartz or quartzite with potassium nitrate as flux. The inlays were sintered before embedding into gilt copper wire filigree. In comparison to the composition proportions in other ancient potash-lime glass, there is no specific percentage of the raw materials in Chinese potash-lime glass, where the ingredients were likely determined by the experience of the craftsman. Compared with existing research on other crowns and their inlays, this study speculates that the crown dates from the Sui dynasty (581–618) or early Tang dynasty (618–649), was made locally by Chinese craftsmen and belonged to the wife of a high official. [ABSTRACT FROM AUTHOR]